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Abstract: The thermal decomposition behavior of survived β-cyclodextrin in its inclusion complex of clove oil is investigated by nonisothermal thermogravimetry (TG) analysis at the heating rates of 5.0, 10.0, 15.0, 20.0 and 25.0Kmin−1. The TG profiles based on mass loss as a function of temperature show a clear trend of increased thermal decomposition temperature with increased heating rate. Gas chromatography coupled to time-of-flight mass spectrometry (GC-TOF-MS) with a programmed temperature heating treatment is performed to experimentally investigate the relationship between procedural decomposition temperature and fragment composition of the sample. The results on the basis of fragment analysis explain the different mass loss of the sample corresponding to different temperatures on the gradient hot stage. [Copyright &y& Elsevier]