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1. Palladium-Catalyzed Reaction of [60]Fullerene with Aroyl Compounds via Enolate-Mediated sp² C-H Bond Activation and Hydroxylation.

Author

Yi-Teng Yan, Wei Gao, Bo Jin, Dong-Shi Shan, Ru-Fang Peng, and Shi-Jin Chu

Abstract

A convenient and highly efficient palladium-catalyzed reaction of [60]fullerene (C60) with aroyl compounds via enolate-mediated C-H activation and hydroxylation has been exploited for the first time to synthesize novel C60-fused dihydrofurans, and rare 1,4-fullerenols. Further functionalization including etherification, and esterification of synthesized 1,4-fullerenols provided efficient access to versatile fullerene derivatives. Moreover, a plausible reaction mechanism leading to the observed products is proposed. [ABSTRACT FROM AUTHOR]

Published
2018
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