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Generally, edge crack of rolled magnesium alloy sheets initiates in the RD (rolling direction)-ND (normal direction) plane and then propagate in the RD-TD (transverse direction) plane. Hence, the Mg-2Zn-1.5Mn (ZM21) alloy sheets with and without crack notch were designed to carry out in-situ tensile experiments under 150 °C (the same temperature of rolling), with the aim to understand their crack propagation mechanism. The scanning electron microscopy (SEM) and electron backscattered diffraction (EBSD) techniques were utilized to reveal microstructural evolution in real time at designated displacements. The results show that the prismatic slip, basal slip, and extension twining play synergistic role in coordinating strain during the tensile process in ZM21 alloy sheet at 150 °C. In both tensile samples with and without crack notch, localized strain is mainly concentrated at relatively fine grain area and the grain boundaries or triple junctions of the grains with large basal Schmid factor (SF) difference, which eventually leads to severe surface roughening and subsequent crack initiation. Compared with the sample without crack notch, the pre-cracked sample exhibits severer deformation at the crack tip due to strain concentration. Strain gradient distribution is observed at the crack tip region in the pre-cracked sample. The crack propagation path of the sample with pre-crack is identified and the underlying mechanism is also discussed.

With neutron diffraction, the local stress and texture of metallic components can be analyzed non-destructively. For both, highly accurate positioning of the sample is essential, requiring the measurement at the same sample location from different directions. Current sample-positioning systems in neutron diffraction instruments combine XYZ tables and Eulerian cradles to enable the accurate six-degree-of-freedom (6DoF) handling of samples. However, these systems are not flexible enough. The choice of the rotation center and their range of motion are limited. Industrial six-axis robots have the necessary flexibility, but they lack the required absolute accuracy. This paper proposes a visual servoing system consisting of an industrial six-axis robot enhanced with a high-precision multi-camera tracking system. Its goal is to achieve an absolute positioning accuracy of better than 50μm. A digital twin integrates various data sources from the instrument and the sample in order to enable a fully automatic measurement procedure. This system is also highly relevant for other kinds of processes that require the accurate and flexible handling of objects and tools, e.g., robotic surgery or industrial printing on 3D surfaces.

Lightweight, high-modulus structural materials are highly desired in many applications like aerospace, automobile and biomedical instruments. As the lightest metallic structural material, magnesium (Mg) has great potential but is limited by its low intrinsic Young's modulus. This paper reviews the investigations on high-modulus Mg-based materials during the last decades. The nature of elastic modulus is introduced, and typical high-modulus Mg alloys and Mg matrix composites are reviewed. Specifically, Mg alloys enhance Young's modulus of pure Mg mainly by introducing suitable alloying elements to promote the precipitation of high-modulus second phases in the alloy system. Differently, Mg matrix composites improve Young's modulus by incorporating high-modulus particles, whiskers and fibers into the Mg matrix. The modulus strengthening effectiveness brought by the two approaches is compared, and Mg matrix composites stand out as a more promising solution. In addition, two well-accepted modulus prediction models (Halpin-Tsai and Rule of mixtures (ROM)) for different Mg matrix composites are reviewed. The effects of reinforcement type, size, volume fraction and interfacial bonding condition on the modulus of Mg matrix composites are discussed. Finally, the existing challenges and development trends of high-modulus Mg-based materials are proposed and prospected.

The hybrid addition of CNTs was used to improve both the strengths and ductility of SiCp reinforced Mg matrix composites. A novel method was developed to simultaneously disperse SiCp and CNTs in Mg melt. Firstly, new CNTs@SiCp hybrid reinforcements were synthesized by CVD. Thus, CNTs were well pre-dispersed on the SiCp surfaces before they were added to Mg melt. Therefore, the following semisolid stirring and ultrasonic vibration dispersed the new hybrid reinforcements well in Mg-6Zn melt. The hybrid composite exhibits some unique features in microstructures. Although the distribution of SiCp was very uniform in the Mg-6Zn matrix, most CNTs distributed along the strips in the state of micro-clusters, in which CNTs were bonded very well with Mg matrix. Most of the CNTs kept their structure integrity during fabrication process. All these factors ensure that the hybrid composite have much higher strength and elongation than the mono SiC/Mg-6Zn composites. The dominant strengthening mechanism is the load transfer effect of CNTs. Apart from grain refinement, the CNTs toughen the composites by impeding the microcrack propagation inside the material. Thus, the hybrid CNTs@SiCp successfully realizes the reinforcing advantage of “1 + 1> 2”.

Objective: To evaluate the diagnostic value of fluorescence in situ hybridization (FISH) in bladder cancer. Methods: We enrolled healthy volunteers and patients who were clinically suspected to have bladder cancer and conducted FISH tests and cytology examinations from August 2007 to December 2008. Receiver operating characteristic (ROC) curve analysis was performed and the area under curve (AUC) values were calculated for both the FISH and urine cytology tests. Results: A cohort of 988 healthy volunteers was enrolled to establish a reference range for the normal population. A total of 4807 patients with hematuria were prospectively, randomly enrolled for the simultaneous analysis of urine cytology, FISH testing, and a final diagnosis as determined by the pathologic findings of a biopsy or a surgically-excised specimen. Overall, the sensitivity of FISH in detecting transitional-cell carcinoma was 82.7%, while that of cytology was 33.4% (p

Abstract Purpose: To evaluate whether low energy shock wave preconditioning could reduce renal ischemic reperfusion injury caused by renal artery occlusion. Methods: The right kidneys of 64 male Sprague Dawley rats were removed to establish an isolated kidney model. The rats were then divided into four treatment groups: Group 1 was the sham treatment group; Group 2, received only low-energy (12 kv, 1 Hz, 200 times) shock wave preconditioning; Group 3 received the same low-energy shock wave preconditioning as Group 2, and then the left renal artery was occluded for 45 minutes; and Group 4 had the left renal artery occluded for 45 minutes. At 24 hours and one-week time points after reperfusion, serum inducible nitric oxide synthase (iNOS), neutrophil gelatinase-associated lipocalin (NGAL), kidney injury molecule-1 (KIM-1), creatinine (Cr), and cystatin C (Cys C) levels were measured, malondialdehyde (MDA) in kidney tissue was detected, and changes in nephric morphology were evaluated by light and electron microscopy. Results: Twenty-four hours after reperfusion, serum iNOS, NGAL, Cr, Cys C, and MDA levels in Group 3 were significantly lower than those in Group 4; light and electron microscopy showed that the renal tissue injury in Group 3 was significantly lighter than that in Group 4. One week after reperfusion, serum NGAL, KIM-1, and Cys C levels in Group 3 were significantly lower than those in Group 4. Conclusion: Low-energy shock wave preconditioning can reduce renal ischemic reperfusion injury caused by renal artery occlusion in an isolated kidney rat model.

Anisotropic behavior is a key characteristic for understanding eccentricity in tubes. In this paper, the effect of using a tilted die during tube drawing on eccentricity, texture, dislocation density, and mechanical properties is shown. Copper tubes were drawn with a ±5° tilted die for two passes. The increase or decrease in eccentricity can be controlled by controlling the angle of the tilted die. Two types of textures have been developed during tube drawing, namely plane strain and uniaxial types. Plain strain type texture is mainly characterized by the β fiber with a dominant copper component {112}. The uniaxial deformation type is dominated by the fiber, as commonly found by wire drawing. Texture sharpness increases with increasing drawing strain, and the texture varies significantly between the maximum and minimum wall thickness. This texture variation between maximum and minimum wall thickness has no significant influence on mechanical properties, which are more or less similar, but the increase in strength after each drawing pass is apparent. The dislocation density is low for the as-received tubes due to recovery and recrystallization. This is consistent with the as-received texture dominated by the cube component {001}. During tube drawing, dislocation density increases as a function of the deformation strain. The variation of dislocation density between the maximum and minimum wall thickness in the tube deformed with −5° tilted die is higher than the variation in the tube deformed with +5° tilted die.

Mg–RE (Dy, Gd, Y) alloys show promising for being developed as biodegradable medical applications. It is found that the hydride REH2 could be formed on the surface of samples during their preparations with water cleaning. The amount of formed hydrides in Mg–RE alloys is affected by the content of RE and heat treatments. It increases with the increment of RE content. On the surface of the alloy with T4 treatment the amount of formed hydride REH2 is higher. In contrast, the amount of REH2 is lower on the surfaces of as-cast and T6-treated alloys. Their formation mechanism is attributed to the surface reaction of Mg–RE alloys with water. The part of RE in solid solution in Mg matrix plays an important role in influencing the formation of hydrides.

Solid-state refrigeration based on the caloric effects is promising to replace the traditional vapor-compressing refrigeration technology due to environmental protection and high efficiency. However, the narrow working temperature region has hindered the application of these refrigeration technologies. In this paper, we propose a method of combined caloric, through which a broad refrigeration region can be realized in a multiferroic alloy, Ni–Mn–Ga, by combining its elastocaloric and magnetocaloric effects. Moreover, the materials’ efficiency of elastocaloric effect has been greatly improved in our sample. These results illuminate a promising way to use multiferroic alloys for refrigeration with a broad refrigeration temperature region.

The present work investigates the influences of microalloying with rare earths on the mechanical properties of magnesium alloys. The amount of each rare earth element is controlled below 0.4 wt.% in order not to increase the cost of alloy largely. The synergic effects from the multi-microalloying with rare earths on the mechanical properties are explored. The obtained results show that the as-cast magnesium alloys multi-microalloying with rare earths possesses a quite high ductility with a tensile strain up to 25–30% at room temperature. Moreover, these alloys exhibit much better corrosion resistance than AZ31 alloy. The preliminary in situ neutron diffractions on the deformation of these alloys indicate that the multi-microalloying with rare earths seems to be beneficial for the activation of more slip systems. The deformation becomes more homogeneous and the resultant textures after deformation are weakened.

In-situ synchrotron diffraction and atom probe tomography (APT) have been used to study the carbon diffusion and redistribution process in austempered ductile iron (ADI) during austempering. The process of carbon content change in bainitic ferrite during different austempering temperatures has been determined quantitatively. The transformation in ADI is controlled by decarburization of supersaturated ferrite and carbide precipitation and has been found to be divided into three stages based on a model developed for bainitic steels by Takahashi and Bhadeshia. The formation, morphology and composition of carbides and carbon clusters in ferrite after austempering have been identified unequivocally by APT. Finally, the relationships of carbon content in ferrite, carbon gap values, and austempering temperatures in the ADI alloy were expressed using empirical equations.

In response to the development of new materials and the application of materials and components in new technologies the direct measurement, calculation and evaluation of textures and residual stresses has gained worldwide significance in recent years. STRESS-SPEC, the materials science diffractometer, which is jointly operated by the Technische Universität München, the Institute of Materials Science and Engineering, Technische Universität Clausthal and by GEMS, Helmholtz-Zentrum Geesthacht, is located at the thermal beam port SR-3 of the FRM II and can easily be configured either for texture analysis or strain measurements.