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3. Relationship between solid state NMR parameters and X-ray structural data in tricadmium phosphates

Author

Aime, S., Digilio, G., Gobetto, R., Bigi, A., Ripamonti, A., Roveri, M., and Gazzano, M.

Subjects
Cadmium -- Research, Phosphates -- Research, Molecular structure -- Research, Chemistry
Abstract

The correlation of the 31P and 113Cd chemical shifts with the crystallographic sites for the six different PO(sub 4)(super 3-) in the unit cell of beta'-tricadmium phosphate has been determined. The method was based on the computation of bond strength at oxygen atoms in phosphate moieties. Spectroscopic analyses of tricadmium phosphates with different degrees of magnesium substitution for cadmium showed the random distribution of magnesium in the cadmium sites, inducing a decrease in the order of structure.

Published
1996

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