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by Lim Che Lau., Thesis (M.Phil.)--Chinese University of Hong Kong, 1996., Includes bibliographical references (leaves 79-84)., Title Page --- p.i, Table of Contents --- p.ii, List of Tables --- p.iv, List of Figures --- p.v, List of Schemes --- p.vii, Acknowledgments --- p.viii, p.ix, Chapter CHAPTER 1: --- INTRODUCTION, Chapter 1.1. --- Historical Background --- p.1, Chapter 1.2. --- FTICR with External Ion Source --- p.2, Chapter 1.3. --- High Mass Analysis in FTICR --- p.4, Chapter 1.4. --- Outline of Present Work --- p.7, Chapter CHAPTER 2: --- INSTRUMENTATION AND EXPERIMENTAL, Chapter 2.1. --- Instrumentation --- p.8, Chapter 2.1.1 --- Ion Source --- p.10, Chapter 2.1.1.1. --- Liquid Secondary Ion Mass Spectrometry --- p.11, Chapter 2.1.1.2. --- Electrospray Ionization --- p.12, Chapter 2.1.2. --- Electrostatic Ion Focusing System --- p.15, Chapter 2.1.3. --- ICR Analyzer Cell and Magnet --- p.18, Chapter 2.1.4. --- Data Acquisition and Handling System --- p.22, Chapter 2.2. --- Experimental --- p.22, Chapter 2.2.1. --- Liquid Secondary Ion Mass Spectrometry --- p.22, Chapter 2.2.2. --- Electrospray Ionization --- p.23, Chapter 2.2.3. --- Nozzle-Skimmer Dissociation --- p.24, Chapter 2.2.4. --- Sustained Off-Resonance Irradiation Collision- Induced Dissociation --- p.24, Chapter 2.2.5. --- Data Acquisition and Processing --- p.27, Chapter 2.2.6. --- Mass Calibration --- p.27, Chapter CHAPTER 3: --- STRUCTURAL CHARACTERIZATION OF TERPYRIDINE-BASED POLYETHER DENDRIMERS AND THEIR IRON(II) METALLOCOMPLEXES BY LIQUID SECONDARY ION MASS SPECTROMETRY AND ELECTROSPRAY IONIZATION MASS SPECTROMETRY, Chapter 3.1. --- Introduction --- p.28, Chapter 3.2. --- Sample Preparation --- p.29, Chapter 3.3. --- Results and Discussion --- p.30, Chapter 3.3.1. --- Liquid Secondary Ion Mass Spectrometry Studies --- p.30, Chapter 3.3.1.1. --- Dendrimers --- p.30, Chapter 3.3.1.2. --- Metallodendrimers --- p.41, Chapter 3.3.2. --- Electrospray Ionization Mass Spectrometry Studies --- p.47, Chapter 3.4. --- Conclusions --- p.53, Chapter CHAPTER 4: --- STUDIES OF LANTHANIDE(III) PORPHYRIN- PHTHALOCYANINE HETEROLEPTIC SANDWICH COMPLEXES USING ELECTROSPRAY IONIZATION, Chapter 4.1. --- Introduction --- p.54, Chapter 4.2. --- Results and Discussion --- p.55, Chapter 4.2.1. --- Molecular Weight Determination --- p.57, Chapter 4.2.2. --- Structural Elucidation --- p.65, Chapter 4.2.3. --- Charge-Transfer Processes --- p.72, Chapter 4.3. --- Conclusions --- p.76, Chapter CHAPTER 5: --- CONCLUSIONS --- p.77, References --- p.79, http://library.cuhk.edu.hk/record=b5888944, Use of this resource is governed by the terms and conditions of the Creative Commons “Attribution-NonCommercial-NoDerivatives 4.0 International” License (http://creativecommons.org/licenses/by-nc-nd/4.0/)