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Grouting is a common and important technique for water bursting prevention in coal mines; the success of grouting in coal mines depends highly on the flowability of grouting materials and the strength of the hardened body as well. In this paper, a series of performance tests, in terms of the water-cement ratio, viscosity, drainage rate, presetting time, final setting time, compressive strength, and permeability were conducted on the cement-fly ash-based grout at various mixture ratios. The evolution of these performances versus different mixture ratios was analyzed; targeting at the reasonable flowability and hardened strength of grouting materials, an optimized mixture ratio was recognized for water bursting prevention in coal mines. Furthermore, the diffusion experiments of optimized grout material were designed taking into account the influence of confining and hydraulic pressure in the porous medium. As a result, the confining and hydraulic pressures have a linear negative correlation with the diffusion distance of grout materials. These results have guiding significance to water bursting prevention in coal mines. [ABSTRACT FROM AUTHOR]