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Here, a novel nanostructured catalyst based on CuO included hallow mesoporous silica spheres (CuO-HMSS) was prepared for synthesis of 1,2,3-triazole compounds. The hallow silica spheres were synthesized via the hydrothermal procedure. The characterization of prepared catalyst was also performed applying several analysis techniques such as TEM and SEM, EDX, XRD, and ICP.Graphical Abstract: CuO active sites in a hollow mesoporous silica shell are stably and efficiently attainable for conversion of precursors to triazole compounds. [ABSTRACT FROM AUTHOR]