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C f -ZrB 2 -SiC is a new composite material with excellent properties for making the next-generation aerospace component. This material is extremely difficult to removal by mechanical machining, and there is a lack of research on feasible secondary processing methods of this composite at present. Micro-EDM is not limited by material hardness, so it is very suitable for machining this material. In this paper, the Material removal mechanisms and processing characteristics of C f -ZrB 2 -SiC by micro-EDM is analyzed. The removal mechanism of composite materials is explored though the discharge crater morphology, and the single-discharge experiments of each phase materials with different medium and different energies are also carried out as a reference. Electrical discharge milling experiments of C f -ZrB 2 -SiC are performed to explore the medium on processing index, and found that the best surface quality and maximum processing efficiency can be realized in kerosene. An experiment with four factors (pulse width, voltage, peak current, capacitance) and three indexes (surface roughness, MRR, TWR) is designed to analyze the C f -ZrB 2 -SiC process characteristics of micro-EDM and the response surface diagram and second-order regression equation are obtained. Milling the C f -ZrB 2 -SiC by electrical discharge according to the optimal combination of surface roughness parameters deduced above, the as-machined surface is analyzed including the surface morphology by SEM, element content by EDS and the surface phase by XRD. The feasibility and advantages of micro-EDM on machining C f -ZrB 2 -SiC are prove. [ABSTRACT FROM AUTHOR]