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1. The synthesis and efficient one-pot catalytic “self-breeding” of asymmetrical NC(sp3)E-hybridised pincer complexes.

Author

Yang, Xiang-Yuan, Tay, Wee Shan, Li, Yongxin, Pullarkat, Sumod A., and Leung, Pak-Hing

Subjects
PHOSPHINE oxides, SULFIDES, CATALYSTS, ALIPHATIC compounds, CATALYSIS research
Abstract

Cyclopalladation of the pyridyl-substituted chiral phosphine sulfide (N–P=S) and oxide (N–P=O) compounds afforded the asymmetric N–C(sp3)*–S and N–C(sp3)*–O pincer complexes. When applied as catalysts in asymmetric hydrophosphination, the newly developed aliphatic pincer catalyst could be recycled over three runs and obtained in large quantities via a one-pot “self-breeding” catalytic protocol. [ABSTRACT FROM AUTHOR]

Published
2016
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