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This study investigated the radiation effects of commercially available medical disposable protective clothing materials under γ irradiation. FT‐IR, contact angle, DSC, OIT, and mechanical properties were used to examine the radiation effects of medical disposable protective clothing materials. The results showed when the radiation dose was less than or equal to 50 kGy, the FT‐IR spectra did not show any changes. However, when the radiation dose reached 70 kGy, new absorption peaks appeared in the infrared spectra of the TS−A and TS−B medical disposable protective clothing materials, indicating chemical changes. Contact angle analysis showed that medical disposable protective clothing materials were hydrophobic and had higher hydrophobicity on the inside than the outside under different packaging and irradiation conditions. Rheological analysis showed that the shear thinning phenomenon of medical disposable protective clothing materials increased significantly with the increase of radiation dose, and good rheological behavior was observed under vacuum packaging conditions when the radiation dose was 30 kGy. The crystallinity and initial crystallization temperature showed the order of vacuum, nitrogen, and air. The oxidation induction time trend was vacuum>nitrogen>air, while the fracture strength trend was nitrogen>vacuum>air. The mechanical properties met the national standard. [ABSTRACT FROM AUTHOR]