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• The two-dimensional temperature field of the tensile process was investigated based on Digital Image Correlation (DIC) technology and cooling heat transfer model. • The reconstructed temperature field is in good agreement with the temperature rise in the tensile process. • The observed trend of increased martensite production is consistent with the simulated predictions. To better understand the tensile fracture behavior and temperature variation during the tension testing of the 316LN at cryogenic temperatures, a two-dimensional temperature field solution method is developed based on two-dimensional strain field measured by the digital image correlation technology combined with the Taylor Quinney coefficient model and the intrinsic model of strain-induced martensitic phase transformation. The method allows for visualization of the strain field and temperature variation of the 316LN austenitic stainless steel at cryogenic temperature. By numerical simulation, the localized temperature elevation of the 316LN is determined to be 13.3 K during the tensile test at 77 K, which is in good agreement with the experimental result of 10.2 K. This model reconstructed the two-dimensional temperature field variation throughout the entire tensile test, which is beneficial for facilitating the analysis of the mutual relation between the mechanical properties and microstructural evolution of the 316LN and other metastable austenitic stainless steels in cryogenic temperatures. [ABSTRACT FROM AUTHOR]

• A Ne-liquefaction system cooled by a G-M cryocooler was developed and the refractive index and transmission of 940 nm infrared in liquid neon were also measured. • The neon gas was liquefied while the condenser chamber temperature was cooled down to 26.7 K and the production rate of liquid neon was 0.52 L/h. • The refractive index and transmittance of 940 nm infrared in liquid neon are 1.103 and 99.85%, respectively. A Ne-liquefaction system cooled by a G-M cryocooler was developed. The heat load and liquefied rate of the system were analyzed theoretically. The neon gas was liquefied over 340 min while the condenser chamber was cooled down to 26.7 K. The gas pressures of the heat exchanger inlet and condenser are directly proportional to its absolute temperature, which decreased with the reduction of cryostat system temperature. The pressure of the heat exchanger inlet decreased from 105 kPa to 100.4 kPa with the pressure of the condenser decreased from 101 kPa to 100.1 kPa. Neon gas with a purity of 99.999% was used in liquefaction and the mass flow is set to 0.173 g/s. The production rate of liquid neon is determined to be 0.52 L/h. The liquid neon was collected in a glass vacuum dewar with a transparent window, which allows to observe the liquid level and conduct the optical tests. The refractive index and transmittance of the 940 nm infrared in liquid neon are 1.103 and 99.85%, respectively. The parameters will provide a valuable database on infrared equipment with liquid neon as a cryogen. [ABSTRACT FROM AUTHOR]

• The sound welded joint was obtained with Ni interlayer for 316L/Cu dissimilar laser welding joint. • No welding defects and spherical particles were formed in the fusion zone. • The average tensile strength of dissimilar welded joint is 408 MPa at 77 K. To improve the quality of welded joints between copper and 316L stainless steel, laser welding with Ni interlayer was carried out. A sound welded joint was obtained and the microstructures as well as mechanical properties were investigated. Results indicate that no welding defects or spherical particles were formed in the fusion zone. The microstructures in the fusion zone were characterized as dendritic grains, and no macroscopic segregation was observed. The welded joint failed at copper base material with an average tensile strength of 408 MPa at 77 K, and ductile fracture mode with dimples on the fracture surface were presented. Moreover, the addition of Ni interlayer prevents formation of welding defects and spherical particles and improves mechanical properties of the joint. [ABSTRACT FROM AUTHOR]

• The internal 3D-view of two Nb 3 Sn strands were detected with a non-destructive way, high-resolution 3D X-ray micro tomography. • The Nb 3 Sn phase of WST strand has a poor crystallinity with high defect density and the filaments of OST strand were connected forming a large Nb 3 Sn bundle. • The higher J c of the OST strand than that of the WST is ensured not only by the overall Nb 3 Sn layers thickness, but also by smaller grain sizes and narrower zone of columnar grains. In the present work, microstructural and microchemical of Nb 3 Sn strands with the internal tin process produced by the Western Superconductor Technology co., Ltd (WST) and Oxford Instruments co., Ltd (OST) were analyzed. The internal 3D-view of two Nb 3 Sn strands were detected with a (sub-)micrometric resolution in a non-invasive, non-destructive way, i.e. high-resolution 3D X-ray micro tomography. The distribution of filaments and voids induced by the functional heat treatment of two strands were investigated. The elements distribution after heat reaction of two strands was investigated through elemental mapping by scanning electron microscope (SEM) and energy dispersive X-ray analysis. The filaments of the WST Nb 3 Sn strand distributed uniformly, whereas the filaments separated with clear copper boundary among filaments. However, the filaments of the OST Nb 3 Sn strand have serious overlap phenomenon and the copper isolation interface was not clear among filaments. In order to investigate the distinction of microstructure, the selected area electron diffraction was also performed by transmission electron microscopy (TEM) and the results indicated that obvious impurities were observed in the Nb 3 Sn phase of the WST strand compared to the OST strand. [ABSTRACT FROM AUTHOR]

• The 0.2% proof stress and ultimate tensile strength at 4.2 K for 35% pre-strained specimens increased respectively around 86% and 18% compared to those of the as-received material. • The elongation at fracture at both RT and 4.2 K decreased for the pre-strained 316LN SS compared to those of the as-received material. • The pre-strained 316LN SS fractured at 4.2 K exhibits a ductile fracture mode. In the present work, influences of room temperature tensile pre-strain on cryogenic tensile properties of 316LN austenitic stainless steel (SS) were investigated. The tensile properties of the 316LN SS with various tensile pre-straining amounts of 15%, 25% and 35% were measured at both room temperature (RT) and liquid helium temperature (4.2 K). Results indicated that both 0.2% proof strength (R p0.2) and ultimate tensile strength (R m) at both RT and 4.2 K of the pre-strained 316LN SS significantly increased compared to those of the as-received material. The R p0.2 and R m at 4.2 K for 35% pre-strained specimens increased around 86% and 18%, respectively, compared to those of the as-received material. However, the elongation at fracture (A) at both RT and 4.2 K decreased for the pre-strained 316LN SS compared to those of the as-received material. The fractured morphologies of the pre-strained 316LN SS were investigated by means of scanning electron microscopy (SEM) and transmission electron microscopy (TEM). Dimples in the surface fractured at both RT and 4.2 K of the as-received and pre-strained 316LN exhibited a ductile fracture mode. Moreover, fractographic results indicated that the pre-strain treatment considerably decreased the ductility at both RT and 4.2 K. TEM analyses revealed that pre-strain treatment at RT led to dislocation accumulation and stress-induced martensite phase occurred at 4.2 K, which interpreted the cryogenic tensile properties of the pre-strained 316LN SS. [ABSTRACT FROM AUTHOR]

• An emissivity measurement system based on radiometric method was designed and built. • The radiation power signal received by detector can be switched by a stepping motor. • The emissivity of the blackbody coating (Nextel 811–21), 304 stainless steel and G10 were measured and discussed. Thermal radiation is a major part of heat transfer in cryogenic systems, especially in vacuum environment. The emissivity of materials is an essential factor of thermal radiation, which is difficult to be precisely predicted by theoretical calculation. Thus, the direct experimental measurement becomes an inevitable, reliable method. In this paper, a preliminary emissivity measurement system using the direct radiometric method was designed and built with a G-M (Gifford-McMahon) cryocooler as the cold source. The sample plate in the apparatus can be cooled to 9.2 K, while the sample thermal radiation shield and the optical path cover can respectively reach 46.7 K and 46.9 K. At present stage, MCT (HgCdTe) detector with an effective bandwidth 2–12 μm was used in this system, which achieved the measurements of emissivities of coating Nextel 811–21, 304 stainless steel and G10 composite from 240 K to 300 K. The reliability of the system was verified by comparing the measurement results with the data already published, and the dependence of the emissivities of these materials on temperature are analyzed. [ABSTRACT FROM AUTHOR]

• Mechanical properties of superconducting magnet insulation materials after reheat. • Strain responses during second Vacuum Pressure Impregnation process. • Monitoring by Fiber Bragg Grating sensors embedded in the insulation layers. • Additional strain introduced by the new added epoxy resin. In large-scale, high-field superconducting magnets used for magnetic confinement fusion, high energy accelerators, and magnetic resonance imaging, the insulating system made from glass fiber reinforced resin-based composites is the key component, which mainly plays the role of mechanical support, fixing and protecting superconducting conductors, as well as electrical insulation. Vacuum Pressure Impregnation (VPI) approach is widely used in the manufacturing of the insulation system. The second curing cycle is generally required after the first VPI and curing process. For example, after the superconducting coil is cured in the mold, the de-molding process requires the superconducting coil to be reheated according the curing temperature. Moreover, for large-scale superconducting magnets, the superconducting coil needs to undergo a second VPI process after the first VPI process to fix the coil in the coil case. In this work, the tensile and shear properties of pure epoxy resin and the glass fiber reinforced resin-based composite, were investigated at both room and cryogenic temperatures and the effect of the second curing cycle on the mechanical properties was analyzed. Additionally, the strain evolution of the Nb-Ti superconducting coil during the second curing cycle was measured using the Fiber Bragg Grating (FBG) sensors embedded in the composite. The results indicate that the second curing cycle will not introduce additional strain to the previously cured resin matrix, but the defective or weak parts of the resin matrix may be affected by the new added epoxy resin and a little extra strain has been observed. [ABSTRACT FROM AUTHOR]

• Fatigue crack propagation behavior of 316LN tungsten inert gas (TIG) weldment and weldment with post weld heat treatment (PWHT) was investigated at liquid helium temperature. • Weldment with PWHT results in the highest fatigue crack propagation resistance, whereas the base material demonstrates the lowest fatigue crack propagation resistance. • The crack featured with a transgranular propagation characteristics for the base material, the weldments without and with PWHT. • More amount of strain-induced martensite near the crack tip in the base material compared to in the as-welded weldment and in the weldment with PWHT. • The strain-induced martensite transformation plays a crucial role in determining the fatigue crack propagation behavior at cryogenic temperature. In the present work, fatigue crack propagation behavior of 316LN tungsten inert gas (TIG) weldment and weldment with post weld heat treatment (PWHT) was investigated at liquid helium temperature. Results indicates that the weldment with PWHT results in the highest fatigue crack propagation resistance, whereas the base material demonstrates the lowest fatigue crack propagation resistance. Microstructure evolution reveals that the fatigue crack propagation is characterized as transgranular fracture for the base material as well as the as-welded weldments and the weldment with PWHT. Moreover, the crack propagation path of the weldments shows a zigzag crack extension, especially for the weldment with PWHT, whereas the crack extension of the base material is relative straight. Electron backscattered diffraction reveals more amount of strain-induced martensite near the crack tip in the base material compared to in the as-welded weldment and in the weldment with PWHT, which is considered to be a crucial factor in the fatigue crack propagation behavior at cryogenic temperature. [ABSTRACT FROM AUTHOR]

• The tree structures, inception probability, growth rates at 77 K were studied. • The Raman spectra of the degradation products within the tree channels at room temperature and 77 K were analyzed. • The effects of oxygen and graphitic carbon on the tree characteristics of epoxy resin were analyzed. The insulation structure which is mainly composed of epoxy resin is a key part of the superconducting magnet system. Due to the special operating environments, superconducting coils must address the challenges of cryogenic liquids and various kinds of high voltages. In this paper, the electrical tree characteristics of epoxy resin at 77 K were investigated. An experimental setup with a partial discharge (PD) device and a cryostat filled with liquid nitrogen (LN 2) was set up. Optical microscopy and confocal Raman spectrometer were applied to investigate the accumulation of degradation products within the tree channels. Each group of samples was tested at a range of AC voltages (50 Hz) from 8 kV rms (root mean square) to 20 kV rms and the PD experiments were carried out at both room temperature and 77 K. The results indicated that the color of electrical trees was darker and the tree structures were more complicated at 77 K compared with those at room temperature. The weak reaction between oxygen and the degradation products within the tree channels was responsible for the darker tree channels at 77 K. The density of electrical trees increased and the damage to materials caused by electrical trees was more serious at 77 K. Meanwhile, the tree inception probability decreased and the tree growth was inhibited obviously at 77 K. It's also revealed that the degradation products within the tree channels were confirmed to be graphitic carbon based on the corresponding Raman spectra. The size of graphitic domains within the tree channels at 77 K was more than 2 times of that at room temperature, which contributed to the tree growth acceleration in the later growth stage at 77 K. [ABSTRACT FROM AUTHOR]

In the present work, a cryogenic mechanical property testing system conduction-cooled by two G-M cryocoolers was developed. The testing sample can be cooled from room temperature to 2.7 K within 7.5 h. The sample was first cooled down to 11.1 K directly by the two G-M cryocoolers and then cooled down to 2.7 K by decompressing the chamber. Instead of liquid helium, the cooling process is characterized by cooling with recycled helium gas as heat transfer medium. The heat load of the system was analyzed and optimizations were adopted in terms of material selections and design. The static load capacity of the system reaches 200 kN and the fatigue load capacity can reach 50 kN. This system can be installed onto an electronic universal testing machine or a fatigue testing machine to characterize static tension, fracture mechanics or fatigue properties at tunable low temperatures. Tensile properties of 316L austenitic stainless steels at 4.2 K were tested with the system and the results were compared with those obtained by cooled using liquid helium, which demonstrates high reliability. [ABSTRACT FROM AUTHOR]

• Mechanical properties of 316LN stainless steel with cryogenic pre-strain were studied at different temperatures (RT, 77 K and 4.2 K). • The pre-strained samples stretched at cryogenic temperature obtain higher mechanical strength. • The samples stretched at 77 K possess higher elongation and hardness than RT and 4.2 K, the mechanism was explained. • The results are attributed to the changes in dislocation density and martensite transformation due to temperature and cryogenic pre-strain. The 316LN stainless steel (SS) used for TF conduits in the ITER must undergo a series of pre-deformation during the fabrication. In order to investigate the variation of mechanical properties of 316LN SS with different temperature and cryogenic pre-strain, the cryogenic pre-strained samples with 0%, 15%, 25%, and 35% pre-strain were prepared and stretched at room temperature (RT), 77 K and 4.2 K, respectively. The yield strength (YS), ultimate tensile strength (UTS), elongation and microhardness of the samples were measured. Besides, the Scanning Electronic Microscopy (SEM) and Transmission Electronic Microscopy (TEM) were applied to observe the microstructure of 316LN SS. The magnetic measurements for the samples were carried out to investigate the volume percent of phase transformation. The results indicate that the YS, UTS and microhardness of 316LN SS are improved by means of cryogenic pre-strain and the decrease of elongation of pre-strained samples is different at different temperatures. All 316LN samples show the ductile fracture. The dislocation of samples promotes by cryogenic pre-strain and hinders by cryogenic temperatures. The martensitic transformation occurs after all pre-strained samples were stretched. The volume percent of α' martensite is minimal at RT and increases dramatically at cryogenic temperatures (77 K and 4.2 K). The combination of dislocation density and martensitic transformation results in changes in the 316LN SS mechanical properties. [ABSTRACT FROM AUTHOR]

• A cryogenic system for measuring electrical properties of insulation materials has been established. • The thermal switch in the cryostat shortens the time of precooling and saves a lot of helium gas. • Two modes in the cryogenic system: 4.2 K mode and 1.65 K mode. • The cryogenic system realizes the coupling of low temperature and high voltage. A cryogenic system has been established to measure electrical properties of insulation materials. The cryostat in the system contains two operating modes: 4.2 K and 1.65 K. A G-M cryocooler is used as cold source in these two modes. In 4.2 K mode, samples were directly cooled by the copper plates connected to the second stage of the cryocooler. In the 1.65 K mode, the helium gas is liquefied. The superfluid 4He (He-Ⅱ) of 1.65 K was obtained by throttling and depressurizing the liquid 4He (He-Ⅰ). The thermal switch in the 1.65 K mode can reduce the precooling time by 11.6 h and saved 22.5 L of helium. The transforming of the two modes is controlled by four threaded rods which are connected to the first and the second stage flange. The electrical test unit is designed, including the breakdown strength test and the flashover characteristics test with the voltage from 0 to 100 kV, which realizes the coupling of low temperature and high voltage. [ABSTRACT FROM AUTHOR]

• The system can quantitatively detect internal and external leakage within a wide range of operating temperatures (20–300 K). • This system using the GM cryocooler instead of cryogen is a benefit for its low operating cost, simple structure, and safe handling. • Five sample valves can be cooled simultaneously and tested in sequence to improve efficiency. • The helium mass spectrometry leak detector was used for its sensitive response and high precision. • The external leakage of the sample valves was detected at LH 2 temperature for the first time. Sealing performance under cryogenic temperatures should be a consideration in the development of a cryogenic valve for use in cryogenic engineering. In the present work, a cryogen-free leak detection system at 20 K to conduct leakage testing of cryogenic valves was developed. The experimental system was composed of a cooling system, a leak detection system, and a PLC (Programmable Logic Controller) system. Compared with the traditional cryogenic leak detection systems, this system using the GM cryocooler instead of cryogen is beneficial for the application for its low operating cost, simple structure, and safe handling. Five valves can be installed simultaneously and tested in sequence. The helium mass spectrometer leak detector is used for its sensitive response and high precision. The reliability of this system was verified by testing the leak rate of the system itself. Three high-pressure cryogenic solenoid valves were tested using helium gas under the pressure varied from approximately 2.5 bar to 80 bar and at both room temperature (300 K) and liquid hydrogen temperature (20 K). The tested valves can be cooled from room temperature to 18 K within 6 h. The test results of the internal leakage rate and the external leakage rate of the samples were discussed. This system will aid in the inspection of many critical cryogenic components such as liquid oxygen and liquid hydrogen valve assemblies for which leakage may lead to serious consequences. [ABSTRACT FROM AUTHOR]

• The epoxy resin has a low viscosity and long pot life. • At 77 K, the epoxy resin offers high tensile strength and modulus. • The superconducting magnet exhibits high shear and compressive strength at 77 K. Superconducting magnet is a key component in magnetic resonance imaging (MRI). In general, vacuum pressure impregnation (VPI) technology is used for insulating system of the superconducting magnet. Performance of the superconducting magnets is affected by the adhesion strength between superconducting wires and resins at cryogenic temperature. In this study, experimental superconducting coil was prepared by modified bisphenol-A type epoxy resin and the VPI technology. Tensile, shear, and compressive properties of the samples cut from the superconducting coil were measured at both room temperature (RT) and liquid nitrogen temperature (77 K), and the bonding properties between the superconducting wire and the resin were discussed. The results show that the resin exhibits low viscosity, long pot life and higher mechanical strength, and it is suitable for impregnating superconducting magnets by VPI technology. Moreover, the shear and compressive strength of the impregnated superconducting magnet at 77 K are significantly higher than that at room temperature, with the increase of 132% in radial compressive strength, 170% in axial compressive strength, 63% in radial shear strength and 70% in axial shear strength, respectively. This study provides references for the design of insulation for superconducting magnet system and the manufacture of insulating materials for MRI superconducting magnets. [ABSTRACT FROM AUTHOR]