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2. Cadmium(ii) and mercury(ii) complexes of an NO2S2-donor macrocycle and its ditopic xylyl-bridged analogue .
3. Donor effect on supramolecular structures of silver(i) perchlorate complexes of macrocycles with O2S2X (X=S, O and NH) donor setsReaction of AgClO4 with L1 in methanol afforded colourless precipitate. The solid was filtered off, and dissolved in acetonitrile. X-ray quality crystals of 1 were obtained by slow evaporation of the solution. Equimolar amount of AgClO4 was added to L2 in acetonitrile and methanol, respectively and slow evaporation of the solution afforded colourless crystals of 2a and 2b suitable for X-ray analysis. Equimolar amount of AgClO4 was added to L3 in acetonitrile and diffusion of diethyl ether into the solution afforded colourless crystals of 3 suitable for X-ray analysis.
4. Donor effect on supramolecular structures of silver(i) perchlorate complexes of macrocycles with O2S2X (X=S, O and NH) donor setsReaction of AgClO4 with L1 in methanol afforded colourless precipitate. The solid was filtered off, and dissolved in acetonitrile. X-ray quality crystals of 1 were obtained by slow evaporation of the solution. Equimolar amount of AgClO4 was added to L2 in acetonitrile and methanol, respectively and slow evaporation of the solution afforded colourless crystals of 2a and 2b suitable for X-ray analysis. Equimolar amount of AgClO4 was added to L3 in acetonitrile and diffusion of diethyl ether into the solution afforded colourless crystals of 3 suitable for X-ray analysis.
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