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Nanoparticle shape strongly affects the thermal-hydraulic behavior of nanofluid-enhanced single-phase natural circulation loop (SPNCL) but is yet to be explored experimentally. Hence, various mono/hybrid nanofluids having dissimilar shaped nanoparticles (Al 2 O 3 +Water, Al 2 O 3 +CuO + Water, Al 2 O 3 +SiC + Water, Al 2 O 3 +MWCNT + Water) with a 0.1% volume concentration, are used in SPNCL to investigate mass flow rate (MFR), heat exchanger effectiveness (HEE) and total entropy generation rate (TEGR). The effect of power input, coolant inlet temperature and loop inclination (both counter-clockwise and clockwise) on transient and steady-state performances are presented. The result reveals that mono/hybrid nanofluid shows enhanced HEE and lower TEGR as compared to base fluids, whereas the MFR may increase or decrease since the performance of SPNCL is significantly impacted by the nanoparticle's shape. Spherical-shaped nanoparticle-dispersed nanofluids show early flow initiation and higher MFR than cylindrical-shaped nanoparticle-dispersed nanofluids. MFR and TEGR rise with higher power input, whereas HEE declines for all working fluids. MFR and TEGR increase as the coolant inlet temperature rises, whereas HEE decreases for all working fluids. The loop inclination decreases the MFR, while it increases the HEE and TEGR. The Counter-clockwise inclination of the loop shows a higher MFR than the clockwise inclination at the same angle of inclination. • Hybrid nanofluids having dissimilar shaped particles are used in natural circulation loop. • Mass flow rate, heat exchanger effectiveness and entropy generation rate are evaluated. • Effect of power input, coolant inlet temperature and loop inclination are investigated. • Spherical-shaped shows early flow initiation and higher flow rate than cylindrical-shaped. • Counter-clockwise inclination shows higher mass flow rate than the clockwise inclination. [ABSTRACT FROM AUTHOR]