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A friction stir butt-welded Ti- and Nb-modified 12 % Cr ferritic stainless steel joint without any defects was successfully produced under low welding heat input. The welding heat cycles, temperature profiles, and degree of plastic deformation during welding were quantitatively evaluated based on the results of a rigid-viscoplastic thermo-mechanically coupled model. Microstructure development in the stir zone (SZ) and thermo-mechanically affected zone (TMAZ) was studied and comparatively analyzed. A fine duplex microstructure containing nearly 62.9 % martensite and 37.1 % ferrite was obtained in the SZ. Undissolved nanometer-sized precipitates during welding played a crucial role in grain refinement in the weld. Retardation of dynamic recrystallization (DRX) occurred in the SZ, and the recrystallized grains were no more than 8% of the materials. The dynamic recovery and continuous DRX experienced by the ferrite grains in the TMAZ of the advancing side were more intense than those on the retreating side, leading to a higher amount of high-angle boundaries and a 20.8 % reduction in dislocation density. The hardness and strength in the SZ apparently increased owing to refined grains and phase transformation. Both the heat-affected zone with a fully ferritic structure and the SZ exhibited superior low-temperature toughness.

Friction stir additive manufacturing (FSAM) was performed successfully using 2 mm thick sheets of 2195-T8 aluminum-lithium alloy. The influence of the tool pin shape and process parameters on the interfacial bonding features among the additive manufactured layers was discussed, and the effects of interfacial defects on the performances of the additive build were analyzed based on microstructures, hardness profiles, and mechanical property evaluations. It is shown that the shape of the tool pin is one of the key factors in influencing the bonding interface between two manufactured layers. The cylindrical pin and the conical pin with three flats are not suitable for the FSAM process since very poor material mixing features are produced along the bonding interface. Although the material mixing degree of bonding interface is obviously improved at the advancing side (AS) interface of the nugget zone (NZ) by using the convex featured pin or the pin with three concave arc grooves, the material mixing degree at the retreating side (RS) interface of the NZ is always insufficient. Meanwhile, the weak-bonding defects along the bonding interfaces could be formed, which are originated from the hooking defects on the RS. The weak-bonding defects are related to the oxides and impurities existing at the original bonding interfaces as well as the insufficient stirring action of the tool pin. The back and forth double passes welding is one of the effective methods to improve the material mixing in the whole NZ and eliminate the hooking defects extending into the NZ. The welding rotation speeds of 800, 900 and 1000 rpm for giving welding speed of 100 mm/min were used in the additive manufacturing processes of 2195-T8 aluminum-lithium alloy, in which the optimum microstructure is obtained with the rotation speed of 800 rpm. The soften degree for the multilayered build is obvious, and the hardness profiles across the different bonding interfaces are always uneven. Meanwhile, compared with the AS interface, the fluctuation of the hardness value at the RS interface is greater. The mechanical properties of the multilayered build are inhomogeneous, and the maximum tensile strength of the multilayered build is only reached the 56.6% of the base metal. The mechanical properties are closely associated with the soften tendency of the material and the degree of the amelioration of weak-bonding defect along the bonding interface.

The effects of friction stir processing (FSP) on microstructures, tensile properties and work hardening behavior of reduced activation ferritic/martensitic steel (RAFM) under different rotation speeds were investigated. The microstructures of FSP samples were examined by scanning electron microscopy (SEM), Electron back scatter diffraction (EBSD) and transmission electron microscope (TEM). Tensile test results show that the FSP samples not only have high strength, but also have good ductility simultaneously. The FSP samples of 150 rpm exhibit the best ductility with an elongation of about 1.5 times that of the base material (BM). The FSP samples of 200 rpm present a good match between strength and ductility, and the ultimate tensile strength (UTS) and total elongation are increased by 77.2% and 34.2%, respectively. FSP samples reveal lower hardening capacity and lower work hardening exponent than BM. As the rotation speed increases, the hardening capacity and the work hardening exponent of the FSP samples gradually decrease. Both BM and FSP samples can be divided into stage III and IV in the Kocks-Mecking type plot of work hardening rate. The FSP samples present the lower absolute slope value at stage III relative to BM. Besides, the FSP samples of 150 rpm and 250 rpm reveal the smallest and largest work hardening rate at stage IV, respectively.

The microstructural characteristics of underwater wet friction taper plug welded joints for API X52 pipeline steel were investigated and tensile strength and facture toughness of the welded joints were experimentally evaluated. The microstructure of welded joints is considerably inhomogeneous. The tensile strength of welded joints shows heterogeneity in thickness direction. All of the tensile specimens taken from upper side of welded joints fracture at base material, while those taken from the bottom are broken at bonding interface or base material. The fracture toughness of welded joints deteriorates seriously, as compared with base material. The welded joints with notches in weld center have higher fracture toughness than those in bonding zone and the axial force has few influences on fracture toughness of welded joints. The bonding zone between plug and base plate should play a role as fissure defect for the whole welded joint, considering that it is tens of microns and much softer than its vicinity. In addition, the coarse grain, quenched martensite and Widmanstatten ferrite in weld region should also be responsible for the reduction of fracture toughness.