1. Study of quasi-two- and three-dimensional ordered porous structures by means of small-angle X-ray scattering in the grazing incidence geometry
- Author
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N. A. Grigoryeva, A. A. Mistonov, Sergey V. Grigoriev, I. S. Dubitskiy, G. A. Valkovskiy, and N. A. Sapoletova
- Subjects
Diffraction ,Materials science ,Solid-state physics ,Small-angle X-ray scattering ,Scattering ,02 engineering and technology ,021001 nanoscience & nanotechnology ,Condensed Matter Physics ,01 natural sciences ,Molecular physics ,Electronic, Optical and Magnetic Materials ,0103 physical sciences ,X-ray crystallography ,Microscopy ,Small-angle scattering ,010306 general physics ,0210 nano-technology ,Structure factor - Abstract
The structure of surface layers of thin metal inverse opals has been studied first by the grazing-incidence small-angle X-ray scattering technique. Contributions of the form factor and structure factor to the small-angle diffraction pattern have been separated using a numerical model of the scattering process. The complementary use of the small-angle X-ray scattering and grazing-incidence small-angle X-ray scattering techniques has provided independent information about the bulk and surface properties of the samples and allowed a type of defect in the investigated structures to be determined. The measurement results have been verified by atomic force microscopy.
- Published
- 2017
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