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3 results on '"Shore, Daniel"'

1. Preparation of 2-Azabicyclo[2.1.1]hexane Hydrochloride

Author

Siu, Michael, primary, Huestis, Malcolm, primary, Liao, Haili, additional, Li, Aimin, additional, Chen, Xingsong, additional, Liang, Kun, additional, Shen, Yang, additional, Liang, Qingfeng, additional, Xu, Kewei, additional, Shore, Daniel, additional, and Villemure, Elisia, additional

Published
2016
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3. Preparation of 2-Azabicyclo[2.1.1]hexane Hydrochloride.

Author

Haili Liao, Aimin Li, Xingsong Chen, Kun Liang, Yang Shen, Qingfeng Liang, Kewei Xu, Shore, Daniel G. M., Villemure, Elisia, Siu, Michael, and Huestis, Malcolm P.

Subjects
AZA compound synthesis, HEXANE, CHLORIDES, ALKYL chlorides, SULFINAMIDES
Abstract

A batchwise, multigram preparation of 2-azabicyclo- [2.1.1]hexane hydrochloride (1·HCl) was developed, delivering a total of 195 grams of material. The key synthetic step involves an intramolecular displacement of a primary alkyl chloride with a tert-butylsulfinamide to forge the [2.1.1]-bicyclic ring system. [ABSTRACT FROM AUTHOR]

Published
2016
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