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1. Synthesis of Acylsilanes via Catalytic Dedithioacetalization of 2-Silylated 1,3-Dithianes with 30% Hydrogen Peroxide.

Author

Masayuki Kirihara, Satoshi Suzuki, Naohiro Ishihara, Kento Yamazaki, Tomomi Akiyama, and Yuki Ishizuka

Subjects
ACYLSILANES, DITHIANE, HYDROGEN peroxide, SODIUM iodide, NIOBIUM
Abstract

Acylsilanes were obtained efficiently from dedithioacetalization of 2-silylated 1,3-dithianes using 30% hydrogen peroxide catalyzed by iron(III) acetylacetonate-sodium iodide. The use of niobium(V) chloride as a catalyst instead of iron(III) acetylacetonate was also effective, except in synthesizing some acyltrimethylsilanes. [ABSTRACT FROM AUTHOR]

Published
2017
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