【Objective】The paper aimed to study the effects of different dilution ratios of carbon dioxide trapping agent on CO2 concentration in ‘Murcott’ tangerine canopy and physiological characteristics of leaves, and to provide theoretical basis and data support for the application of carbon dioxide trapping agent in citrus production practice.【Method】In the study, six-year-old trifoliate orange rootstock ‘Murcott’ tangerine was used as test material, and the leaves were sprayed with 1∶100, 1∶150, 1∶200 dilution ratio carbon dioxide trapping agent, and the same amount of water was applied as the control. The change characteristics of CO2 concentration in citrus canopy were investigated, and the leaf morphological characters, chlorophyll content, photosynthetic characteristics and non-structural carbohydrate were measured. 【Result】Compared with CK, the CO2 concentration in the three dilution ratios of carbon dioxide trapping agent increased significantly(P<0.05), and increased by 1.63%(treatment T1), 1.94%(treatment T2) and 1.78%(treatment T3), respectively. The Chla and Chl(a+b) contents in T2 and T3 treatments increased significantly compared with CK on 2 June(P<0.05). The peak values of T1 treatment were leaf width, louver fresh weight, Pn daily mean, Tr daily mean, Fo, Fm, Fv/Fm and Fv/Fo, among which Pn daily mean, Fo, Fm, Fv/Fm and Fv/Fo showed significant differences compared with CK(P<0.05);T3 treatment showed peak values in Gs daily mean, Ci daily mean, leaf length, length-width ratio, leaf area and leaf dry weight, only leaf length and leaf dry weight were significantly different from CK(P<0.05). Soluble sugar content was decreased and starch content was increased in the three groups treated with carbon dioxide trapping agent. On May 13, Soluble sugar and starch contents of T3 treatment were significantly different from those of CK(P<0.05). 【Conclusion】Carbon dioxide trapping agent could increase the concentration of CO2 in the canopy of ‘Murcott’ tangerine, producing a positive response to the physiological characteristics of leaves, increasing the accumulation of biomass and chlorophyll in leaves, effectively alleviated the ‘nap’ phenomenon of ‘Murcott’ tangerine, and changed the ratio of photosynthetic products. Different dilution ratio of carbon dioxide trapping agent had different response to physiological characteristics of ‘Murcott’ tangerine leaves. [ABSTRACT FROM AUTHOR]