1. Study on Identification of Nickel-containing Solid Waste Based on Multi-technology Combination.
- Author
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PAN Shenglin, ZHA Yanqing, DAI Dongqing, HOU Jianjun, FENG Yahui, ZHENG Jianming, YAN Wenxun, and XU Renfu
- Subjects
SOLID waste ,NICKEL ores ,X-ray fluorescence ,X-ray spectroscopy ,FLUORESCENCE spectroscopy ,X-ray diffraction ,LEAD oxides ,IRON-nickel alloys - Abstract
The micro-morphology, chemical composition and phase composition of nickel-containing material samples are analyzed by using ultra depth of field microscopy, X-ray fluorescence spectroscopy and X-ray diffraction. Combined with the characteristic analysis of nickel ore and nickel slag, the attribute identification of solid waste is realized. The results show that the micro structure of sample 1 is fluffy and broken floe, the pH value is 4.30, and the acid characteristic is remarkable. The main phases of sample 1 are SiO
2 , FeO (OH), PbO2 , etc. The residual content of sulfur in the sample reaches 14.7%, and the contents of Pb and As far exceed the limit of harmful substances. There are voids on the surface of sample 2, showing obvious black scorch marks. The main phases of sample 2 are Mg2 SiO4 and Fe3 O4 . The converted content of MgO in the sample far exceeds the standard limit of nickel concentrate. Comprehensive analysis of the appearance, physical properties, microscopic morphology, phase composition, chemical composition of the two materials, the two materials do not have natural mineral characteristics, inferred that the material 1 may come from the wet smelting slag produced by the laterite nickel ore in the sulfuric acid leaching process, and the material 2 may be the smelting slag or converter slag produced by the smelting process of nickel-containing minerals by pyrotechnic smelting, which belongs to solid waste. [ABSTRACT FROM AUTHOR]- Published
- 2022
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