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1. Efficient and stereoselective synthesis of thiosulfinates from disulfide using cumene hydroperoxide in the presence of titanium-based catalyst systems.

Author

Sun, Pengju, Huang, Jiansheng, Xu, Jinyi, and Yu, Niefang

Subjects
*CATALYSTS, *DISULFIDES, *HYDROPEROXIDES, *OXIDIZING agents, *OXIDATION
Abstract

An efficient and stereoselective procedure of oxidizing disulfide to thiosulfinate 2a using CHP as the oxidant and economically available Ti(O-i-Pr)4/L-DET/H2O as catalysts were developed. The reaction went smoothly under mild conditions with synthetic useful yield and the workup for obtaining the final product is quite convenient. [ABSTRACT FROM AUTHOR]

Published
2019
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