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Abstract This study aims to characterise the so-called Sialkoti paper used to produce Pahari drawings preserved today in the Wereldmuseum in Leiden (Netherlands) (WML). These works originate from the Punjab Hills in India (today Himachal Pradesh) and are commonly known as ‘Pahari miniature paintings’. The paper upon which these drawings are executed is said to have been produced in Sialkot during the eighteenth and nineteenth centuries when papermaking was an integral part of an overall regional economy correlated with other sectors such as agriculture and the textile industry. Although the term Sialkoti refers to identified papermills in Sialkot (now Pakistan), the paper from this region is yet to be subjected to a systematic study. This article therefore explores the paper(s) in question through macro- and microscopic observations of structure, pulp and fibres. The study of historical sources, complemented by the analysis of paper samples and fibre identification, has revealed that the pulp would have been prepared from a variety of manufactured products using different technologies, such as rags, cloth, mats, rope and other plant-based materials made from local bast fibres which, once tattered, were recycled to prepare the pulp. Microscopic study reveals that a variety of fibre combinations under different conditions and processing steps were used, in particular sunn hemp fibre (Crotalaria juncea L.), a plant species that has until now rarely been identified in historical paper. In addition, the presence of kenaf and jute fibres, as well as a significant quantity of cotton fibres, have also been demonstrated. To overcome the lack of comparative materials, our work was supported by a comparative study of several materials made from sunn hemp now held in the Ethnobotany Collection at Kew Gardens. Samples were taken from these materials and provided useful reference micrographs for the identification of the WML samples. The quality of the paper used by Pahari artists, as well as the raw materials available and their processing, are discussed in detail. Putting all the data, including technical and historical information into perspective, we conclude that the Pahari artists used a paper of inferior quality compared to other types of paper used for other purposes such as the creation of illuminated manuscripts in the Punjab plains. This study therefore provides useful analytical and material evidence that complements previous historical, technical and anthropological studies.

This paper proposed phytoliths as promising for identifying and distinguishing sources of fibre in Chinese handmade papers. For an initial methodological exploration, two types of Raw Xuan (unprocessed Xuan paper) and the two plant materials used in making them—namely rice straw and bark from blue sandalwood (Pteroceltis tatarinowii Maxim.)—were collected. The dry ashing method was used to extract phytoliths from Raw Xuan and its plant materials. The results can be summarized as follows. First, phytoliths characteristic of rice (Oryza sativa) were abundant in both rice straw and Raw Xuan. By looking for rice phytoliths, it is possible to tell whether or not rice straw fibre is used in a particular paper. Second, hair cell phytoliths were observed in considerable quantities in blue sandalwood bark, but absent in the examined papers. Heat experiments showed that phytoliths in blue sandalwood were resistant to long-term heat and they would unlikely be eliminated when exposed to the heat in papermaking (with heat source barely above 200°C). It is hypothesised that they dissolved while cooked in an alkaline pH (limewater). Further studies are necessary to understand whether phytoliths in blue sandalwood—while cooked in limewater—undergo morphological changes and, if yes, how.

This paper proposed phytoliths as promising for identifying and distinguishing sources of fibre in Chinese handmade papers. For an initial methodological exploration, two types of Raw Xuan (unprocessed Xuan paper) and the two plant materials used in making them—namely rice straw and bark from blue sandalwood (Pteroceltis tatarinowii Maxim.)—were collected. The dry ashing method was used to extract phytoliths from Raw Xuan and its plant materials. The results can be summarized as follows. First, phytoliths characteristic of rice (Oryza sativa) were abundant in both rice straw and Raw Xuan. By looking for rice phytoliths, it is possible to tell whether or not rice straw fibre is used in a particular paper. Second, hair cell phytoliths were observed in considerable quantities in blue sandalwood bark, but absent in the examined papers. Heat experiments showed that phytoliths in blue sandalwood were resistant to long-term heat and they would unlikely be eliminated when exposed to the heat in papermaking (with heat source barely above 200°C). It is hypothesised that they dissolved while cooked in an alkaline pH (limewater). Further studies are necessary to understand whether phytoliths in blue sandalwood—while cooked in limewater—undergo morphological changes and, if yes, how. [ABSTRACT FROM AUTHOR]

This study investigates the earliest surviving Tibetan paper, from the Dunhuang cave library, using paper fibre analysis combined with codicological, palaeographical and textual information. The hypotheses tested by this method concern the regional origins and production centres of early Tibetan paper and methods for dating this material. Using overlapping typologies, we classify a sample of manuscripts into coherent groups, relating them to particular 'book cultures'. By linking three main manuscript groups to different geographical regions, we offer new insights into an important manuscript collection, and show that the method of overlapping typologies has the potential to yield further insights. [ABSTRACT FROM AUTHOR]

One hundred and sixty-nine fibre samples from books in the Korean collection and 68 samples from books in the Japanese collection at the British Library were analysed. A further 15 samples of Korean paper from a private collection were also examined. The analysis confirmed that most of the papers contained mulberry species (Moraceae family) as the main papermaking material, and other materials, such as hemp, rice straw and reed, which have been commonly known as supplements to traditional Korean papermaking. However, 15 Korean papers and one Japanese paper dating betweenad 1498 and 1798 appeared to include coniferous wood fibres. This substantial find supports a previous single find of a coniferous wood fibre in Korean paper. The dates of most of these papers containing wood fibres precede the use of wood pulps in European paper. [ABSTRACT FROM AUTHOR]

Abstract: This work focuses on the study of paper and textiles used in the binding of a series of manuscripts that share some specific characteristics that lead us to speculate on the possibility of a transitional codicological typology from the Arabic to the Christian book in Al-Andalus during the 15th century. The books we analyzed belong to the collection of the Historical Archive of Malaga, the Archive of Sacromonte Abbey, in Granada, the School of Arabic Studies and the Library of P.P. Escolapios, also in Granada. Paper physical study was performed by microscopic and spectroscopic techniques. A routine and objective method, Fourier Transform Infrared (FTIR) spectroscopy, was employed and proved to be a useful technique for the characterization of cellulosic fibres, main component of paper from the boards and the envelope flap pasteboards, and the fabric lining from the cover. The results of our research will help us to date, identify and study the evolution of the techniques, proving that the materials and innovations of the Italian paper manufacturing processes were perfectly known in the south of modern day Spain, before the Christian Reconquest. [Copyright &y& Elsevier]

Simple, rapid staining analytical methods with visual color assessment are the most used in practice, but they involve problems including subjective error, low accuracy, qualitative results, and the necessity of using many kinds of stains and a great deal of morphology information for correct identification. A method of objective fiber identification using color vectors of a microscan from stained fibre digital photography is described in this report. A model set of cellulose fibres was prepared: groundwood; sulphate pulp; Whatman paper; and rag fibres. The objective micro-colorimetric method, using RGB (red, green, blue) vectors with discriminatory analysis, reduced the number of stains to 1; requires no morphological information; and the discriminatory power (dp,) of this approach is up to 95 to 100% of correctly identified unknown samples with one color vector R or B. A dp value of 100% was achieved when using 2-P or 3-P combinations of R, G, and B. [ABSTRACT FROM AUTHOR]

Hop (Humulus lupulusL.) is an ancient perennial crop plant, native to the Northern Hemisphere. The archaeological evidence dates back to at least the sixth century ad in Europe. Hop has been used for beer brewing, in sleeping draughts, as bedding and for antibacterial purposes. Less known is that hop fibres have also been used for textiles and paper. However, it is difficult to distinguish hop from other bast fibres. Here, we present a set of fibre features, which, when found together in an archaeological/historical material within a European context, provide a strong indication that the fibres are hop. [ABSTRACT FROM AUTHOR]

Bast fibres have been commonly used as a textile material in Northern Europe since Neolithic times. However, the process of identifying the different species has been problematic, and many important questions related to their cultural history are still unanswered. For example, a modified Herzog test and the presence of calcium oxalate crystals have both been used in identification. In order to generate more reliable results, further research and advancement in multi-methodological methods is required. This paper introduces a combination of methods which can be used to identify and distinguish flax (Linum usitatissimum), hemp (Cannabis sativa), and stinging nettle (Urtica dioica). The research material consisted of reference fibres and 25 fibre samples obtained from 12 textiles assumed to be made of nettle. The textiles were from the Finno-Ugric and Historical Collections of The National Museum of Finland. The fibre samples were studied by observing the surface characteristics and cross sections with transmitted light microscopy, and by using a modified Herzog test with polarized light, in order to identify the distinguishable features in their morphological structures. The study showed that five out of 25 samples were cotton, 16 nettle, one flax, and one hemp. Findings from two samples were inconsistent. The results show that it is possible to distinguish common north European bast fibres from each other by using a combination of microscopic methods. Furthermore, by utilizing these combined methods, new and more reliable information could be obtained from historical ethnographic textiles, which creates new vistas for the interpretation of their cultural history. [ABSTRACT FROM AUTHOR]

Cotton (Gossypium species) was used as textile fibre already in the early Indus culture, and since then it has been cultivated in Tropical and Subtropical regions around the whole planet. The species G. hirsutum is nowadays the dominant cotton crop with more than 90% of the world market, while G. barbadense, G. herbaceum and G. arboreum combined, the other cultivated species of Gossypium genus total a minor part of world's cotton production. Even in places where cotton was not cultivated, it could be an important trade item and income source for local textile centres, with the imported raw cotton lint being spun, woven and for some part exported from such sites around the globe. This all occurred far away from Finland, until changes brought by the development of long-distance trade and the Industrial Revolution. Based on archaeological finds, cotton as a textile material reached Finland relatively late, in the early Middle Ages. The article focuses on the problematic nature of identifying these cotton finds: whereas modern cotton fibres are easy to identify, the archaeological finds can at first sight be confused with bast or un-degummed silk fibres. This issue will be approached through reviewing recent Finnish cotton finds in heritage textiles. Additionally, the article examines whether the four cultivated cotton species could be differentiated using both classical and newly developed fibre identification methods, such as optical microscopy methods, a Scanning Electron Microscope (SEM), Fourier-transform infrared spectroscopy (FTIR) or Wide-Angle X-ray Scattering (WAXS). [ABSTRACT FROM AUTHOR]

Plant fibres have been used since ancient times in numerous applications ranging from nets and basketry to textiles for clothing. A proper identification of plant fibre remains in archaeological excavations provides important information about resource exploitation and agriculture. In order to identify plant fibres, a series of fibre features-cross-section diameter, lumen diameter, dislocations (nodes), cross markings, cross-section shape and lumen shape-have been defined and characteristic traits of these features for different fibre types established. How suitable these traits really are for fibre identification has been a matter of debate. To resolve this issue, we have performed a systematic investigation of typical textile bast fibres: flax, nettle and hemp. We have investigated cross-section diameter, lumen diameter, dislocations (nodes) and cross markings using standard compound, white light transmission microscopy. Our investigations show that all the traits that are considered characteristic for one type of plant fibre can also, on occasion, be found in other types. This demonstrates that an investigation of the traits listed above is not sufficient to ensure a correct identification of the plant fibre material; in particular, when only a small amount of material is available. This is often the case in archaeological excavations. [ABSTRACT FROM AUTHOR]

In Finland, the earliest remains of a Christian church and cemetery date to the Late Iron Age (800–1150/1300 AD) and have been excavated in Ravattula Ristimäki, in Kaarina, southwestern Finland. In this study, seven assumingly plant fibre textile samples from individual inhumation graves were analysed to identify their materials. The aim of the study was to investigate the possibilities of identifying archaeological plant fibre samples using a three-stage procedure by observing the surface characteristics, microfibrillar orientation and cross section of the fibres via transmitted light microscopy (TLM). The identification process was based on such a TLM characterisation. Additionally, parts of the samples were studied with X-ray microtomography (micro-CT) and wide-angle X-ray scattering (WAXS) to test the possibilities of using the X-ray methods in research and to identify bast fibre textiles. Both flax and nettle were found in the samples, indicating a preference for these two fibre plants in Late Iron Age Finland. [ABSTRACT FROM AUTHOR]

Abstract: Identifying and distinguishing between natural textile fibres is an important task in both archaeology and criminology. Wool, silk and cotton fibres can readily be distinguished from the textile bast fibres flax, nettle/ramie, hemp and jute. Distinguishing between the bast fibres is, however, not easily done and methods based on surface characteristics, chemical composition and cross section size and shape are not conclusive. A conclusive method based on X-ray microdiffraction exists, but as the method requires the use of a synchrotron it is not readily available. In this paper we present a simple procedure for identifying the above mentioned textile bast fibres. The procedure is based on measuring the fibrillar orientation with polarised light microscopy and detecting the presence of calcium oxalate crystals (CaC2O4) in association with the fibres. To demonstrate the procedure, a series of fibre samples of flax, nettle, ramie, hemp and jute were investigated. The results are presented here. An advantage of the procedure is that only a small amount of fibre material is needed. [ABSTRACT FROM AUTHOR]

Hop (Humulus lupulus) has been used in Scandinavia since at least the ninth century AD, as documented through archaeological findings and written, historical records. The written records are mainly focused on the use of cone-shaped flowers for beer brewing and medical purposes, but there are also records, for example, from the famous Swedish botanist Carl von Linne, who mentions the use of hop fibres for textile production. However, until now no experimental investigations have been published on the use of hop fibres in cultural heritage objects. A major reason for this has been the lack of a suitable characterization method. Hop is a bast fibre, just as flax and hemp and bast fibres cannot be distinguished from each other by simple optical inspection. Recently a new identification method for hop fibres was published by the authors of this article. Here we apply the new method in an investigation of two Swedish cultural heritage objects: (i) a woman’s garment from the nineteenth century, which was labelled as having an upper section made from coarse linen and a bottom section made of hemp and hop and (ii) a textile fragment from an eighteenth-century textile sample book, which was labelled as being made from hop. We show that the woman’s garment is made with hop and hemp fibres and the textile fragment from the textile sample book is made with hop. Our work provides the first direct proof that hop fibres were used for textiles in the past. [ABSTRACT FROM AUTHOR]

Simple, rapid staining analytical methods with visual color assessment are the most used in practice, but they involve problems including subjective error, low accuracy, qualitative results, and the necessity of using many kinds of stains and a great deal of morphology information for correct identification. A method of objective fiber identification using color vectors of a microscan from stained fibre digital photography is described in this report. A model set of cellulose fibres was prepared: groundwood; sulphate pulp; Whatman paper; and rag fibres. The objective micro-colorimetric method, using RGB (red, green, blue) vectors with discriminatory analysis, reduced the number of stains to 1; requires no morphological information; and the discriminatory power (dp,) of this approach is up to 95 to 100% of correctly identified unknown samples with one color vector R or B. A dp value of 100% was achieved when using 2-P or 3-P combinations of R, G, and B.