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In this paper, the mathematical modeling and simulation of the automatic control of the quintuple effect of evaporation of a sugar mill "El Palmar" in Venezuela is made. The multiple effect consist of 5 evaporators Robert type, with equal characteristics, connected in series. Starting from the desired operating conditions and control requirements: level in each evaporator vessel, cane syrup concentration and pressure in the fifth evaporator vessel using mass balances, balance on solids for each evaporator and energy to the barometric condenser is present at the output of the fifth vessel, the nonlinear model of the process is obtained, resulting in a system of multiple inputs and multiple outputs, with strong interactions between variables. In the design of the system of the automatic process control, we are interested in maintaining the variables that characterize the performance of it and they are regulated in an operating point; we proceed to linearize the model around an equilibrium point, resulting in a new model in terms of the variables variations around an environment from that point. Then, it is processed the model obtained in terms of input and output relations, based on the characterization of it in terms of variables and transfer relationships in the complex frequency domain. Finally, the evaporation process is simulated, establishing the adequacy of the model to the real process. [ABSTRACT FROM AUTHOR]