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2. Sequential [3+2] annulation reaction of prop-2-ynylsulfonium salts and hydrazonyl chlorides: synthesis of pyrazoles containing functional motifs

Author

Jiankang Zhang, Jiaan Shao, Zhaoxiao Wu, Huajian Zhu, Rangxiao Zhuang, Linghui Zeng, Chong Zhang, Jia Tingting, Shourong Liu, and Tao Shi

Subjects
Annulation, Chemistry, Materials Chemistry, Metals and Alloys, Ceramics and Composites, General Chemistry, Combinatorial chemistry, Catalysis, Surfaces, Coatings and Films, Electronic, Optical and Magnetic Materials
Abstract

A novel sequential [3+2] annulation reaction has been developed using prop-2-ynylsulfonium salts and hydrazonyl chlorides, affording a series of pyrazoles with functional motifs that can be post modified in the preparation of various drugs or drug candidates. Further transformation and gram-scale operations could also be achieved efficiently.

Published
2021

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