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Abstract: During excavations in the huge ditched enclosure of Valencina de la Concepción (Seville, Spain), the main centre from the first hierarchical framework-settlement in the Guadalquivir Valley, a pit with remains of a context for producing ivory artefacts, dating from the first half of the 3rd millennium BC, was discovered in the large metallurgical nucleate workshops. Scientific (Optical Microscopy, FIRT and Raman Spectroscopy, C/N Isotope Ratio Mass Spectrometry) analyses revealed that the ivory belonged to Asian elephants and the archaeological study, which was made in a specialized workshop context. In this paper we present the archaeological context, the study of the ivory artefacts and the state of research on ivory in the Lower Guadalquivir Basin during the 3rd millennium BC. In a parallel way, this paper discusses the significance of this workshop context in the configuration and function of the long distance circulation of raw material and the specialized craft areas in the first political centres. [Copyright &y& Elsevier]

Abstract: Since 2005 we have been utilizing accelerator mass spectrometry (AMS) 14C dating in research on calcium oxalate crusts associated with open air rock art of the Iberian Peninsula. In this paper we present two dates linked with three eye-idol pictographs at Abrigo de los Oculados (Henarejos, Cuenca, Spain). Radiocarbon ages for these motifs agree with the expected iconography-based archaeological chronology. Such oxalate dates could provide an independent basis for evaluating chronological theories for post-Palaeolithic sites, designated in the UNESCO World Heritage List as Rock Art of the Mediterranean Basin on the Iberian Peninsula. [Copyright &y& Elsevier]

Abstract: The analysis of trade and their implications for understanding social interaction is a major research question of prehistoric research in Europe. Variscite is a rare mineral that offers an excellent opportunity to study trade and exchange patterns in prehistoric Europe through proveniencing of source material. In this paper we discuss the exploitation and exchange of variscite at Pico Centeno mining district during the Copper Age. XRF, XRD, and FTIR analyses of the mineral recovered at Pico Centeno mining district during archaeological survey provides a baseline mineral signature for the source and sub-sources, which were then compared to other Iberian sources and to 44 green beads from 8 megalithic tombs from two different regions, in order to test ‘provenance postulate’ and distribution models. Mineral sampled during survey at Pico Centeno mining district turned out to be pure variscite phases, while extremely varied for the studied green beads: variscite, muscovite, talc or chlorite. On testing ‘provenance postulate’ we have focused on compositional comparison of Pico Centeno’s variscite with reference from various geological sources of Western Europe. We found that the concentrations of trace elements do not allow us to establish the origin of the beads, as traditionally claimed, due to the strong natural variability on minor and trace elements of the sources. Instead we found after FTIR analysis, that different proportions of phosphate species, which results in P/Al ratios higher than 1, arose during the genesis of the variscite deposits and resulted from the associated pH and nature of the host-rocks, modifying the concentrations of PO4 3−, H2PO4 − and HPO4 2−. Thus, the P/Al atomic ratio should be an indication of provenance as it is established during mineral genesis. This issue has not been addressed in any of the other studied sources where this ratio seems to be ≈1. [Copyright &y& Elsevier]