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Additive Friction Stir Deposition (AFSD) is a solid state, bulk, metal additive manufacturing technology that seeks to replace certain castings and forgings wherever it is economically feasible among other applications. Critical to its deployment is an in depth understanding of how the solid state deposition process effects engineering alloys used in relevant applications. In this work, an aerospace aluminum alloy 7075 is evaluated both in the as deposited and heat treated condition via age hardening studies and tensile testing. It is found that an embrittlement phenomena occurs that is sensitive to processing parameters and quench rate during heat treatment. Through the use of SEM, TEM, and APT the embrittlement phenomena has been linked to excessive grain boundary precipitation caused by a combination of shear induced mixing and shear induced segregation which allow for the formation of phases at grain boundaries that are slow to dissolve, leaving the grain boundary in a non-equilibrium solute rich state. Critical to this process is the role of dispersoid particles, which are modified by shear processes which provide high energy spots for thermally stable precipitate nucleation. Removal of these dispersoid particles by an alloy modification had been shown to eliminate the embrittlement effect after depositing in a condition where embrittlement is expected for the unmodified 7075. Further work demonstrates the different relationships between processing conditions and the degree of embrittlement for three different tool types. Beyond the implications of the particular alloy studied, this work highlights the fundamental concepts involved when a manufacturing process operates at high strain rates and total strains which can be used for the design of alloys meant for AFSD.

Wire-based metal additive manufacturing utilizes the ability of additive manufacturing to fabricate complex geometries with high deposition rates (above 7 kg/h), thus finding applications in the fabrication of large-scale components, such as stamping dies. Traditionally, the workhorse materials for stamping dies have been martensitic steels. However, the complex thermal gyrations induced during additive manufacturing can cause the evolution of an inhomogeneous microstructure, which leads to a significant scatter in the mechanical properties, especially the toughness. Therefore, to understand these phenomena, arc-based additive AISI 410 samples were fabricated using robotic gas metal arc welding (GMAW) and were subjected to a detailed characterization campaign. The results show significant scatter in the tensile properties as well as Charpy V-notch impact toughness data, which was then correlated to the microstructural heterogeneity and delta (δ) ferrite formation. Post-processing (austenitizing and tempering) treatments were developed and an ~70% reduction in the scatter of tensile data and a four-times improvement in the toughness were obtained. The changes in mechanical properties were rationalized based on the microstructure evolution during additive manufacturing. Based on these, an outline to tailor the composition of “printable” steels for tooling with isotropic and uniform mechanical properties is presented and discussed.