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The extraction of the phosphate ore produces a high amount of waste causing serious environmental problems. This waste, termed as phosphate washing waste, was filtered and dried at 105°C for 24h to remove the water. The dried waste was milled and then sieved in a 100μm sieve. The resulting phosphates washing waste (PWW) particles size are below 70μm. The phosphate washing waste was calcined at 700°C and 900°C. Both calcined and uncalcined waste were investigated with X-ray fluorescence (XRF), X-ray powder diffraction (DRX), Fourier transform infrared (FTIR), simultaneous differential thermal and thermogravimetric analyses (DTA-TG) and particle size analysis. This waste was activated with sodium hydroxide (NaOH) and sodium silicate in order to produce geopolymeric materials. The influence of replacing PWW by 15% of metakaolin was also study. The results show that the highest compressive strength is obtained with metakaolin. The results also showed that compressive strength decreased with the increase of NaOH concentration.