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Start Over Author "Carnaroglio D." Publication Type Magazines
1 results on '"Carnaroglio D."'

1. Fast TiO2-catalyzed direct amidation of neat carboxylic acids under mild dielectric heatingElectronic supplementary information (ESI) available: IR spectra in the 3800–1100 cm−1range and NMR spectra of the characterization of product. See DOI: 10.1039/c4cy00038b

Author

Calcio Gaudino, E., Carnaroglio, D., Nunes, M. A. G., Schmidt, L., Flores, E. M. M., Deiana, C., Sakhno, Y., Martra, G., and Cravotto, G.

Abstract

The development of green protocols for amide bond formation is a major socioeconomic goal for chemical and pharmaceutical industries and an important challenge for academic research. We herein report a protocol for the quantitative conversion of carboxylic acids and amines to form amides at 100 °C in the presence of a TiO2powder catalyst, under monomodal microwave irradiation. The sustainability of the process appears to be augmented by the ease with which the catalyst is recycled.

Published
2014
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