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The mineralization mechanism responsible for the fossilization of archaeological textiles in close proximity to metal artifacts presents a sophisticated preservation process at both macro and micro levels. This study examines archaeological textiles dating from 2200 BC to AD 1900, sourced from three distinct archaeological sites. The focus is on understanding the microstructural degradation of fibers within a specific burial environment and the preservation achieved through mineralization. These archaeological fibers of archaeological textiles exhibit morphological preservation in the immediate vicinity of copper-based objects. Utilizing tools such as a digital camera, scanning electron microscopy with energy dispersive spectroscopy (SEM–EDS), high-resolution synchrotron-based microtomography (μCT), and enzyme-linked immunosorbent assay (ELISA), we examined fiber morphology, conducted elemental analysis, identified fiber types, and analyzed fiber characteristics. Our findings reveal the presence of smooth-surfaced wools and silks, fibers covered with calculi, and fiber impressions—all subjected to mineralization. These mineralized fibers can be categorized into three distinct stages of mineralization, each exhibiting varying carbon content. We inferred a correlation between mineralization rate and carbon content while also identifying mineralization density distribution on these textiles. Lastly, this study provides insights into the preservation states of textiles across three different mineralization stages, enriching our understanding of the deterioration of organic archaeological material. [ABSTRACT FROM AUTHOR]

Yingpan, Xinjiang, was an important site on the Silk Road of China. A large number of precious objects with exquisite patterns have been excavated from this site, and they provide valuable physical evidence for the study of the cultural exchanges between China and the rest of the world. The conservation methods applied to a pair of cloud pattern-painted boots excavated in Yingpan, Xinjiang, are introduced in this paper, and the various factors influencing the repair process are explained. The results show that an oil-in-water emulsifier with contaminant removal and antibacterial functions effectively softened the hardened and deformed ancient leather. The use of near infrared spectroscopy (NIR) to evaluate the dosage of the softening agent can prevent excessive use of softening agents on historical leathers. A silk crepeline method was used to influence the physical reinforcement of the boots without affecting their appearance. It improved the fiber strength of the ancient textiles. This article is a good reference for conservators seeking to repair ancient leather products with textiles. [ABSTRACT FROM AUTHOR]

Keywords: Pomelo peel; extraction; cellulose nanofibrils; lemon juice hydrolysis; ; ; ; ; EN Pomelo peel extraction cellulose nanofibrils lemon juice hydrolysis ZH 8415 8428 14 11/21/22 20221220 NES 221220 Introduction The large-scale production of the agricultural products in the recent decades has brought significant economic benefits to the humanity; however, the negative impact of the agricultural residues on the environment cannot be ignored (Ullah, Kumar Sharma, and Dhingra et al. [45]). It was observed that with the gradual processing stages, the impurities such as hemicellulose and lignin were removed, and the relatively pure cellulose material with the chemical structure of natural cellulose was obtained. However, in this study, these peaks are observed to be separated after ball milling, which shows that the high-energy ball milling is able to effectively peel off hemicellulose and lignin around cellulose to further purify the extracted cellulose. This is owing to the effective removal of ash, grease, and non-cellulose entities on the surface of cellulose during the extraction process, thus, exposing the cellulose material inside the raw sample. [Extracted from the article]

Precious organic cultural relics are easily affected by temperature, humidity, and harmful gases in the environment, resulting in embrittlement, fading, mildew, moth damage and other aging forms. An energy-saving and environmentally friendly material is needed to stabilize humidity and adsorb harmful gases in the environment. In this paper, with an intelligent adjustment function, functional paper containing sepiolite and tourmaline natural minerals was successfully prepared. The component of 80 % of wingceltis and 20 % of straw in dry pulp as main raw material was conducive to the desorption of water molecules. As favorable structure inside functional paper, the adsorption point and the adsorption contact area increased by the rough surface of fiber bundles, the addition of sepiolite and the ordered molecular chains of copolymers destroyed. So, the relative humidity could be adjusted to 55 % ± 3 within 2 hours and was stable with functional paper. At the same time, 1.11 ppm sulfur dioxide and 2.98 ppm ammonia could be effectively adsorbed in 10 and 12 h, respectively, by 1 g of paper in a 5 L container. The pH of the paper was adjusted to neutral with tourmaline, even if the pH was changed by acidic or alkaline gas absorption. Therefore, for long-term organic cultural relic preservation, preparing a constant-humidity and clean environment is of great significance. This is possible through this paper. [ABSTRACT FROM AUTHOR]