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Thermal/vegetable oil-based mono/hybrid nanofluids (Nano-oils) may be potential working fluids in single-phase natural circulation loops for medium temperature applications due to their favorable thermophysical properties (high thermal expansion coefficient and low viscosity) and high Prandtl number; however, not studied yet. Hence, the present study investigates the different nano-oils in a natural circulation loop. Therminol-VP1 and soybean-based mono/hybrid nano-oils with different nanoparticles (Al 2 O 3 , CuO, SiC, and MWCNT) are used at a volume fraction of 0.1%. The influence of power input and loop inclination on the energy-exergy performance parameters (Effectiveness, Entropy generation rate and Induced mass flow rate) are presented. The use of nano-oil shows enhanced heat exchanger effectiveness and lower entropy generation rate, whereas the induced mass flow rate may increase or decrease depending on nanoparticle shape and power input. Al 2 O 3 +MWCNT nano-oil exhibits superior performance, with a maximum mass flow rate reduction of 8%, effectiveness enhancement of 36%, and entropy generation reduction of 20% as compared to base oil. Therminol-VP1 shows quick flow establishment than soyabean oil. The usage of nano-oil is more beneficial at the higher power input. Loop inclination reduces the mass flow rate while increasing the effectiveness and entropy generation; however, mass flow reduction is much lower for counter-clockwise inclination. • Hybrid nano-oils having dissimilar shaped particles are used in natural circulation loop. • Mass flow rate, heat exchanger effectiveness and entropy generation rate are evaluated. • Effect of power input and loop inclination are investigated for a medium temperature range. • Therminol-VP1 shows quick flow establishment and better performance than soyabean oil. • Counter-clockwise inclination shows higher mass flow rate than the clockwise inclination. [ABSTRACT FROM AUTHOR]