1. Graphite resistive heated diamond anvil cell for simultaneous high-pressure and high-temperature diffraction experiments.
- Author
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Hwang H, Bang Y, Choi J, Cynn H, Jenei Z, Evans WJ, Ehnes A, Schwark I, Glazyrin K, Gatta GD, Lotti P, Sanloup C, Lee Y, and Liermann HP
- Abstract
High-pressure and high-temperature experiments using a resistively heated diamond anvil cell have the advantage of heating samples homogeneously with precise temperature control. Here, we present the design and performance of a graphite resistive heated diamond anvil cell (GRHDAC) setup for powder and single-crystal x-ray diffraction experiments developed at the Extreme Conditions Beamline (P02.2) at PETRA III, Hamburg, Germany. In the GRHDAC, temperatures up to 2000 K can be generated at high pressures by placing it in a water-cooled vacuum chamber. Temperature estimates from thermocouple measurements are within +/-35 K at the sample position up to 800 K and within +90 K between 800 and 1400 K when using a standard seat combination of cBN and WC. Isothermal compression at high temperatures can be achieved by employing a remote membrane control system. The advantage of the GRHDAC is demonstrated through the study of geophysical processes in the Earth's crust and upper mantle region., (© 2023 Author(s). Published under an exclusive license by AIP Publishing.)
- Published
- 2023
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