Search

Hot compression tests were performed with strain rates (0.01–10 s−1) and temperatures (850–1150 °C). The power law relationship between the critical stress and critical strain and Zener–Hollomon parameters was determined by θ-σ curves. Microstructure was investigated by electron backscattered diffraction. The results showed that the flow behavior and microstructure of 35CrMo steel was affected by ultrasonic-assisted casting. The activation energy of non-ultrasonic and ultrasonic-assisted 35CrMo steel were 410 ± 9.9 and 386 ± 9.4 kJ/mol, respectively, and the activation energy of ultrasonic-assisted specimens was reduced by 6%. In addition, the ultrasonic-assisted treatment refines the grains to some extent and makes the softening process of ultrasonic-assisted samples progress faster, which promoted the development of dynamic recrystallization and the production of Σ3 boundaries. The discontinuous dynamic recrystallization was the main DRX nucleation mechanism of the 35CrMo steel. [ABSTRACT FROM AUTHOR]

The effect of deep cryogenic treatment on microstructure and wear resistance of LC3530 Fe-based powder laser cladding coating was investigated in this paper. The cladding coating was subjected to deep cryogenic treatment for the different holding times of 3, 6, 9, 12, and 24 h, followed by tempering at room temperature. Microstructure of the cladding coating was observed by optical microscope (OM) and the microhardness was measured by the Vickers-hardness tester. The wear was tested by ball and flat surface grinding testing conducted on the material surface comprehensive performance tester. The wear scars were analyzed using a non-contact optical surface profiler and scanning electron microscope (SEM). The results showed the grain size of cladding coating after 12 h of deep cryogenic treatment was significantly reduced by 36.50% compared to the non-cryogenically treated cladding coating, and the microhardness value increased by approximately 34%. According to the wear coefficient calculated by the Archard model, the wear resistance improved about five times and the wear mechanism was micro-ploughing. The deep cryogenic treatment could enhance the wear resistance of the cladding coating by forming a wear resistant alloy compound and higher surface microhardness. [ABSTRACT FROM AUTHOR]

Hot deformation experiments of as-cast 35CrMoV steel, with strain rates of 0.01 s−1 and 10 s−1, deformation temperatures of 850, 950, and 1050 °C, and an extreme deformation reaching 50%, were carried out using a Gleeble-3810 thermal simulator. Electrochemical corrosion experiments were conducted on the deformed specimens. The microstructure was observed by optical microscope (OM), and the corrosion morphology and corrosion products of the specimens were investigated by scanning electron microscopy (SEM), energy disperse spectroscopy (EDS), confocal laser scanning microscopy (CLSM), and X-ray diffraction (XRD) techniques. The results show that the grain size increased gradually with an increase in the deformation temperature at the same strain rate, whereas the corrosion resistance deteriorated. At the same deformation temperature, the grain size becomes smaller as the strain rate increases, which enhances the corrosion resistance. This is mainly attributed to the fine grains, which can form more grain boundaries, increase the grain boundary area, and accelerate the formation of the inner rust layer at the beginning of corrosion. Moreover, fine grains can also refine the rust particles and enhance the bonding strength between the inner rust layer and the matrix. The denseness and stability of the inner rust layer increases as the corrosion process progresses, thereby improving corrosion resistance. [ABSTRACT FROM AUTHOR]