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1. Site-Selective Double and Tetracyclization Routes to Fused Polyheterocyclic Structures by Pd-Catalyzed Carbonylation Reactions

Author

Nicola Della Ca, Bartolo Gabriele, Nicolò Sarti, Francesco Pancrazzi, Raffaella Mancuso, Carla Carfagna, Alessia Bacchi, András Stirling, Mirco Costa, Paolo Pio Mazzeo, Pancrazzi F., Sarti N., Mazzeo P.P., Bacchi A., Carfagna C., Mancuso R., Gabriele B., Costa M., Stirling A., and Della Ca' N.

Subjects
Amide, Letter, 010405 organic chemistry, Chemistry, Organic Chemistry, Regioselectivity, Carbonylation, 010402 general chemistry, 01 natural sciences, Biochemistry, Combinatorial chemistry, Chemical reaction, 0104 chemical sciences, Catalysis, Cyclization, Site selective, Molecule, Urea, Physical and Theoretical Chemistry
Abstract

In this contribution, we report novel palladium-catalyzed carbonylative cascade approaches to highly functionalized polyheterocyclic structures. The Pd-catalyzed carbonylative process involves the regioselective insertion of one to three CO molecules and the sequential ordered formation of up to eight new bonds (one C-O, two C-C, five C-N). The exclusive formation of six-membered heterocycles is elucidated by detailed modeling studies.

Published
2020

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