1. Demonstration of a chamber for strain mapping of steel specimens under mechanical load in a hydrogen environment by synchrotron radiation
- Author
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Matthew J. Connolly, Jun-Sang Park, Elizabeth S. Drexler, Damian S. Lauria, Andrew J. Slifka, and Peter E. Bradley
- Subjects
010302 applied physics ,Diffraction ,Materials science ,Mechanical load ,Hydrogen ,chemistry.chemical_element ,Synchrotron radiation ,Advanced Photon Source ,02 engineering and technology ,Paris' law ,021001 nanoscience & nanotechnology ,01 natural sciences ,Synchrotron ,law.invention ,chemistry ,law ,Aluminium ,0103 physical sciences ,Composite material ,0210 nano-technology ,Instrumentation - Abstract
We demonstrate a hydrogen gas chamber suitable for lattice strain measurements and capturing radiographs of a steel specimen under a mechanical load using high energy synchrotron x-rays. The chamber is suitable for static and cyclic mechanical loading. Experiments were conducted at the 1-ID-E end station of the Advanced Photon Source, Argonne National Laboratory. Diffraction patterns show a high signal-to-noise ratio suitable for lattice strain measurements for the specimen and with minimal scattering and overlap from the gas chamber manufactured from aluminum. In situ radiographs of a specimen in the hydrogen chamber show the ability to track a growing crack and to map the lattice strain around the crack with high spatial and strain resolution.
- Published
- 2018
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