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Cyclic interactions between rocks and water have general significance and are particularly relevant to engineering failures and geohazards. A comprehensive investigation of the multi-scale deterioration effects and mechanisms of cyclic wetting-drying on rocks can contribute to better engineering applications, but the probabilistic characterization of rock mass properties under cyclic wetting-drying remains a problem due to the difficult-to-test parameters and limited data. Numerous experiments on rock samples of argillaceous siltstone subjected to cyclic wetting-drying of Yangtze River water demonstrate progressive alteration of rock properties on multiple scales, including changes in mineralogy, grain structure, computed tomography, microporosity, and complexity of micropores, with calcite and albite being the most active minerals. The uniaxial compression strength and indirect tensile strength decrease exponentially with the cyclic number, while the Young's modulus increases. Considering the probabilistic characteristics of the geological strength index, the probabilistic mechanical properties of rock mass of studied argillaceous siltstone are then estimated through the generalized Hoek-Brown criterion. The results indicate that the uniaxial compression strength and indirect tensile strength of rock mass both follow lognormal distributions, while the Young's modulus follows a skewed distribution. Long-term strength parameters of rock and rock mass can also be determined as they exhibit exponential trends with the cyclic number. During the cyclic wetting-drying process, the water-rock interactions produce progressive changes in mineral compositions, microstructures, and micropores; with the accumulation of variations of physical properties, defects grow and develop into weak zones, thus the mechanical properties of argillaceous siltstone are significantly weakened. Investigations of the wetting-drying effects on the geological strength index and probabilistic characteristics of rock sample properties are recommended to accurately evaluate rock mass properties affected by cyclic wetting-drying. • Argillaceous siltstone is treated by cyclic wetting-drying of Yangtze River water. • Dissolution of calcite and albite results in the synergistic evolution of rock properties. • Micropores with a diameter greater than 100 μm become predominant. • Probabilistic properties of rock mass strength under cyclic wetting-drying are evaluated. • Long-term strength of the rock mass is evaluated through the exponential fitting. [ABSTRACT FROM AUTHOR]

As a consequence of seasonal variations in groundwater level and reservoir water level, natural rocks generally experience the cyclic wetting-drying process, in which the change in microstructure becomes a critical factor leading to the deterioration of the macro-physical and mechanical properties of rocks. However, it remains a great challenge to quantitatively characterize the microstructures of rock, especially during the wetting-drying process. In this study, a systematic experimental investigation involving multiple techniques (mercury injection capillary pressure (MICP), computer tomography (CT), scanning electron microscope (SEM), and pores (particles) and cracks analysis system (PCAS) software package-based image analysis) were conducted to study the microstructure of sandstone subjected to cyclic wetting-drying. The results show that sandstone experiences increasing microporosity during the cyclic wetting-drying process, with progressive changes in micro grains, defects, and micropore structure and morphology. The pore compositions gradually change into a bimodal distribution with dominating small-medium pores (10 nm-10 μm) and large pores (>10 μm). Eventually, connected crack networks and large-scale fractures develop. There is a strong correlation between the microporosity values evaluated by CT and MICP, indicating the capacity of describing the micropore compositions ranging from 0.03 to 0.78 mm. Besides, comparisons of the three techniques (i.e., MICP, CT, and SEM) and evolution mechanisms of sandstone microstructures are further discussed. • Sandstone microstructures under cyclic wetting-drying are studied via multiple techniques. • Pore area, complexity, and microporosity gradually increase, and defects grow. • Micropores have a bimodal distribution with small-medium pores and large pores being dominant. • Micropores show morphological anisotropy in three dimensions. • CT agrees with MICP in describing micropore compositions ranging from 0.02 to 1 mm. [ABSTRACT FROM AUTHOR]

The salts contained in water can gradually accumulate in pore networks of rocks under wetting-drying cycles, which could cause rock deterioration. The salt-induced damage under this cyclic process can result in dynamically evolving mechanical and hydraulic properties of the rock, which is relevant to many rock-related engineering activities and geological hazards. In this study, the structure damage and permeability evolution of Three Gorges Reservoir (TGR) sandstone subjected to wetting-drying cycles with salt solution were investigated by a series of multiscale experiments. The results showed that the salt solution has a significant impact on the physical properties of TGR sandstone during the wetting-drying process. With increasing wetting-drying cycles, two typical macroscopic damage modes in form of surface peeling and internal cracking were observed. Various physical parameters indicated that the internal structure of the TGR sandstone experienced two stages: 1) Salt accumulation and new crack formation stage and 2) Crack propagation stage. This variation also profoundly affected the permeability of the TGR sandstone. Specifically, the permeability of TGR sandstone decreased slightly at first due to blocked seepage channels by crystals before cycle 5, followed by a slow growth until the 15th cycle and a rapid increase after the 15th cycle. Cubic and exponential functions showed good performances to describe the evolution features of permeability with porosity and wetting-drying cycles, respectively. The deterioration mechanism was further elucidated by an evaporation test. This test indicated that the salt solution was more likely to crystallize in narrow pores and expectedly exert pressure enough to crack the pores, contributing to the structure damage feature and the permeability enhancement. These findings and results in this study deepen our understanding of salt-induced rock deterioration mechanism under the wetting-drying cycles and would be meaningful for rock engineering safety and geological disaster forecast in complex groundwater environments. • Structure damage of TGR sandstone by salt solution under wetting-drying cycles is systematically revealed. • Permeability enhancement of TGR sandstone is functionalized by porosity and wetting-drying cycle. • Salt-induced deterioration mechanism is elucidated by its crystallization features of location and pressure. [ABSTRACT FROM AUTHOR]