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The aim of the work was to produce laminated structures consisting of Ti–6Al–4V alloy and AA2519 plates and to investigate their microstructure and mechanical properties with an emphasis on the role of an additional AA1050 interlayer. Explosive welding was selected as a joining technology. The microstructure and chemical composition of the explosively joined samples were investigated. Mechanical properties were evaluated in the tensile testing and by microhardness analysis. The results demonstrated that explosive welding is an effective way to produce Ti/Al laminates. Both Ti6Al4V/AA2519 and Ti6Al4V/AA1050/AA2519 laminated plates exhibit good quality of bonding without voids and major delamination. The explosive welding produced metallurgical bonding with a nanostructured zone consisting of Al 3 Ti and Al 2 Ti phases. This zone is thicker in the joint with additional AA1050 interlayer when compared to direct AA2519/Ti6Al4V bonding. In the latter, SEM and STEM analysis reviled the presence of net-like structure in the collision zone. Advanced EDX analysis shows the enrichment of grain boundaries in copper. The formation of this structure is widely discussed. In addition, the explosive welding introduces large plastic deformation which induces the process of grain refinement in aluminium plates. Tensile testing confirms that joining section is not the weakest element of the cladded plates. [ABSTRACT FROM AUTHOR]

Abstract: The nanostructure and mechanical properties of ferritic-austenitic duplex stainless steel subjected to hydrostatic extrusion were examined. The refinement of the structure in the initial state and in the two deformation states (ε=1.4 and ε=3.8) was observed in an optical microscope (OM) and a transmission electron microscope (TEM). The results indicate that the structure evolved from microcrystalline with a grain size of about 4μm to nanocrystalline with a grain size of about 150nm in ferrite and 70nm in austenite. The material was characterized mechanically by tensile tests performed in the two deformation states. The ultimate strength appeared to increase significantly compared to that in the initial deformation stages, which can be attributed to the grain refinement and plastic deformation. The heterogeneity observed in microregions results from the dual-phase structure of the steel. The results indicate that hydrostatic extrusion is a highly potential technology suitable for improving the properties of duplex steels. [Copyright &y& Elsevier]

The microstructure of Mo was significantly refined by high pressure torsion to verify its irradiation tolerance in comparison with its micrograined counterpart. After deformation microhardness increased from 231 Hv0.2 for a microgarined sample to 542 and 558 Hv0.2, respectively after one and five rotations. Concurrently, the grain refinement was observed, as the grain size decreased with the increase of the deformation degree down to 480 and 110 nm, respectively for one and five rotations. Subsequently, deformed Mo and a micrograined one were irradiated by He ions to the dose of 8 × 1016/cm 2 to verify their potential application as fusion mirrors. Irradiations were followed by reflectivity measurements in the 300–2400 nm range with a dual beam spectrometer. The measurements revealed that the applied dose causes a decrease in total reflectivity of the micrograined sample, whereas the total reflectivity of deformed samples decreases by additional 2.5%. Nanohardness measurements, detailed microscopy observations using focused ion beam and scanning transmission electron microscope as well as positron annihilation spectroscopy investigations were performed to elucidate changes in the microstructure and understand the different mechanisms of bubble creation after irradiation in micrograined and high pressure torsion processed samples. • Micrograined and HPT-processed Mo were irradiated with He ions. • HPT of Mo leads to a less significant increase in nanohardness after irradiation. • HPT of Mo contributes to higher density of nanocracks after irradiation. • Positron annihilation spectroscopy was used to characterize vacancies. [ABSTRACT FROM AUTHOR]