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The safe and efficient development of ultra-deep shale gas deeper than 4500 m is closely related to the comprehensive evaluation of the mechanical behavior, brittleness and anisotropy characteristics of reservoir rocks under in-situ stress conditions. However, the above-mentioned information about ultra-deep shale is rarely reported. This study aims to fill this gap by systematically investigating the mechanical and anisotropic characteristics of cores, with 0° and 90° bedding orientations, from different layers in the vertical depth of 4900–4930 m, under confining pressure of 110 MPa. Furthermore, a new brittleness index with three parts related to brittle failure, i.e., the energy storage performance in the pre-peak stage, the performance of elastic energy used to maintain the post-peak failure, and the severity of the energy released during the post-peak stage, all of which are physically meaningful, was proposed. Subsequently, the index was validated and applied to the brittleness evaluation of ultra-deep reservoir rocks. The brittleness was evaluated in the following descending order: black shale of Longmaxi Formation ＞ gray-black shale of Wufeng Formation ＞ limestone of Baota Formation. Overall, the Wufeng- Longmaxi Formation shale still exhibits brittle failure under such high confining pressure, while the Baota Formation limestone exhibits quasi-ductile failure, which is consistent with the phenomenological behavior of cores. Further, various experimental techniques have been employed to study the brittle and quasi-ductile failure mechanisms of reservoir rocks. The anisotropy evaluation results show that the anisotropy degree of the mechanical and brittleness parameters corresponding to the deep formation is significantly lower than that of the shallow formation. The anisotropy degree of strength and deformation parameters (Young's modulus, Poisson's ratio) is closely related to the content of quartz and clay minerals, respectively. The above results are expected to provide data support and theoretical guidance for the development of deep and ultra-deep shale gas in the southern Sichuan region of China. • The mechanical characteristics of ultra-deep reservoir rocks in the vertical depth range of 4900–4933 m are reported. • The influence of the bedding effect on the mechanical behavior of reservoir rocks under high confining pressures is studied. • A new three-part brittleness index in which each part has a clear physical meaning related to brittle failure is proposed. • The brittle and quasi-ductile failure mechanisms of reservoir rocks under high confining pressures are revealed. [ABSTRACT FROM AUTHOR]

Highlights • Two different thermal cycling treatments were applied to granite samples. • Both slow cooling and rapid quenching induced damage to granite samples. • Rapid quenching has a more significant effect on granite samples due to thermal-gradient cracking. • The thermal deterioration mechanisms due to different thermal cycling were revealed by optical microscope observations. Abstract Two different types of thermal cycling treatments (slow heating followed by slow cooling or rapid quenching) were carried out on the granite samples in the present research. The responses of physical, mechanical and transport properties of the granite after various thermal cycling treatments were compared and analyzed. Non-destructive tests (mass, volume, longitudinal wave propagation and permeability) and destructive tests (uniaxial compression and Brazilian splitting) were utilized to characterize these properties. Variations of all the properties demonstrate that thermal cycling (heating and cooling) can induce damage in the samples. Mass, density, P-wave velocity, UCS, Young's modulus and tensile strength decrease, whilst volume and permeability increase with rising temperature. Additionally, the results also demonstrate the importance of cooling method. Rapid quenching has a more significant effect on granite samples, showing lower density, P-wave velocity and strength, but greater permeability, which is due to the generation of thermal gradient cracks. Moreover, the difference between P-wave velocity and UCS of slow cooling and those of rapid quenching increases with temperature up to 500 °C, which can be attributed to the more significant thermal shock cracking induced by higher temperature-gradient stress in the samples during rapid quenching. The microstructural analyses from thin sections show that microcracking in granite subjected to thermal cycling treatments was induced in different severity depending on peak temperature and cooling method. [ABSTRACT FROM AUTHOR]

• The mode-I fracture toughness of granite at high temperature was tested in real time. • The increase in temperature in the low-temperature range universally toughens the rock. • Heat treatment method affects the mode-I fracture toughness of granite. • The temperature threshold of granite fracture toughness at real-time high temperature is 200 °C. • Fracture characteristics of granite at high temperature are similar to those after cooling. The mode-I fracture toughness of semicircular bend granite specimens at high temperature was tested in real time, and the failure specimens were examined using X-ray computed tomography. The results showed that with increasing temperature, the fracture toughness increased from room temperature (20 °C) to 200 °C, then decreased beyond 200 °C. Quasibrittle failure was observed up to 500 °C, followed by plastic characteristics at 600 °C. The cracks tended to propagate along the boundaries of mineral crystals. With increasing temperature, the main cracks became rougher and tended to propagate perpendicular to the tensile stress, and more branch cracks formed. The increase of temperature within a certain range had toughening effect on a variety of rocks and temperature-treatment method affected the mode-I fracture toughness of granite. Compared with the mode-I fracture toughness after cooling to room temperature, the temperature threshold of mode-I fracture toughness of granite at real-time high temperature was higher. The results provide guidance to determine fracture toughness and stability for high-temperature rock engineering. [ABSTRACT FROM AUTHOR]