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In this article, the electrochemical monitoring of phenol (Ph) in water by using a nanostructured MnO2-modified screen-printed carbon electrode (MnO2-SPCE) is reported. MnO2 nanoparticles were synthesized by the redox-precipitation method. Morphological, textural, and microstructural characteristics were investigated by scanning electron microscopy (SEM), X-ray diffraction, Raman, Brunauer–Emmett–Teller (BET) surface area, and pore volume analyses. Electrochemical properties of the modified MnO2-SPCE electrode have been investigated by cyclic voltammetry and linear sweep voltammetry. The detection of Ph in water by the developed sensor was exploited using square wave voltammetry and chronoamperometry. The sensor showed good characteristics, such as simple fabrication, low cost, good sensitivity, stability, reproducibility, and selectivity, against inorganic analytes and other phenolic compounds. The reported results demonstrated the great potential of nanostructured MnO2 in developing high performances electrochemical sensors to be utilized in the field of environmental pollution monitoring. [ABSTRACT FROM AUTHOR]

This article describes a simple though extremely effective sensor for acetone monitoring in the breath. The sensor is capable of monitoring the presence of acetone at parts per million (ppm) concentrations, thus being suitable for a diabetes diagnosis. It has a dimension of $3 {\,\,\mathrm {mm}} \times 6 {\,\,\mathrm {mm}}$ and a cost of less than one dollar. The small dimensions allow one to greatly limit the power required to increase its temperature, and its high selectivity with respect to other gases present in the breath reduces the risk of false-positive responses. The sensor is based on a thin alumina substrate on which platinum strips are deposited on both faces. A thin Nb2O5 layer with a nanometric thickness provides the required sensitivity and selectivity. Sensor prototypes have been characterized by field emission scanning electron microscopy (FESEM) and X-ray photoelectron spectroscopy (XPS) and proved an inherent linear response up to a few ppm of acetone. [ABSTRACT FROM AUTHOR]