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A compact high-power four-port circulator aiming to simplify the conventional, complex, and bulky injection-locking magnetron system is proposed. To reduce the performance deterioration and the risk of ferrite rupture under long-term high-microwave-power condition, the method of breaking a monolithic ferrite into three discrete ferrites in a conventional three-port circulator is proposed. To miniaturize the size and cost of the four-port circulator, a butterfly-shaped waveguide structure is proposed, with a stub inserted into the cavity at the central point and with no connecting waveguide. Multiphysics simulation results show that the temperature coefficient of variation (COV) at the surface of the discrete ferrites is 12.4% lower than that of a monolithic ferrite circulator, with input microwave power of 10 kW. The size of the proposed four-port waveguide circulator is 27% less than the assembly of two three-port circulators, and way smaller than a conventional differential phase shift circulator (DPSC). The simulated and measured S-parameters match well, and the measured power capacity of the fabricated circulator is higher than 3 kW (limited by the experimental condition). A magnetron is successfully locked using only one designed compact circulator. The research in this paper promotes the development of injection-locking magnetron and provides a design example for the compact, high-power circulator. [ABSTRACT FROM AUTHOR]

A wideband superdirective array, composed of a two-element circular monopole configuration, is introduced. The monopoles are placed in close proximity, facing each other on a metal ground. To ensure good matching at high frequencies, two pairs of elliptical patches are added to the sides of the monopoles, enhancing the surface current of the circular patch for wideband performance. To achieve equal amplitude excitation and the desired phase difference, a wideband power divider with a phase shifter is designed to feed the antenna array. Simulation and measurement results demonstrate that the proposed wideband antenna array, operating within the frequency range of 2.94–7.93 GHz, exhibits a maximum directivity of 8.36–10 dBi, with an antenna efficiency ranging from 47.86 to 83.18% across the bandwidth. The proposed array has the advantages of miniaturization, high directivity and wideband operation and can be widely used in various portable wireless communication systems, including WLAN (5.05–5.9 GHz), ISM (5.725–5.875 GHz), 5G communication (3.3–3.8 GHz), etc. [ABSTRACT FROM AUTHOR]

In this paper, an oblique aperture ridge waveguide operating at 2450 MHz is proposed, and, using the ridge waveguide, a permittivity measurement system is constructed which can measure the permittivity of materials during microwave heating. The system calculates the amplitudes of the scattering parameters by using the forward, reflected and transmitted powers of the power meters, and it reconstructs the permittivity of the material by combining the scattering parameters with an artificial neural network. The system is used to measure the complex permittivity of mixed solutions of methanol and ethanol with different ratios at room temperature, and the permittivity of methanol and ethanol with increasing temperature, from room temperature to 50 °C. The measured results are in good agreement with the reference data. The system allows simultaneous measurement of the permittivity with microwave heating and provides real-time, rapid changes in the permittivity during heating, avoiding thermal runaway and providing a reference for applications of microwave energy in the chemical industry. [ABSTRACT FROM AUTHOR]

Microwave-assisted chemical reactions have been widely used, but the overheating effect limits further applications. The aim of this paper is to investigate the coupling degree of the electromagnetic field and thermal field in microwave-heating chemical reactions whose polarization changes as the reactions proceed. First, the entropy-balance equation of microwave-heating polar-molecule reactions is obtained. Then, the coupling degree of the electromagnetic field and the thermal field in microwave-heating polar-molecule reactions is derived, according to the entropy-balance equation. Finally, the effects of reaction processes on the degree of coupling are discussed. When the time scale of the component-concentration variation is much greater than the wave period during the chemical processes, the degree of coupling is sufficiently small, and the electric and thermal fields are considered as weakly coupled. On the other hand, the degree of coupling may change during the reactions. If the absolute value of the coupling degree becomes larger, due to the change in component concentration, this will lead to a transition from weak coupling to strong coupling. [ABSTRACT FROM AUTHOR]

Microwave-driven electrodeless ultraviolet (UV) lamps have the advantages of high efficiency and high power. However, the conventional microwave system is slightly oversized, which restricts the use of the lamp in a narrow space. A miniaturized microwave-driven electrodeless UV lamp based on a coaxial slot antenna was developed in this study. First, the structure of slots was optimized using a finite-difference time-domain algorithm such that high efficiency of radiated energy could be achieved. Second, a complex model based on the Drude model and the electromagnetic theory was established to simulate the interaction between the microwave and UV lamps. The efficiency and uniformity of the UV lamps were analyzed. Finally, an experimental system was built, and the computed results agreed well with the simulation results. The efficiency of the miniaturized microwave-driven electrodeless UV lamp reached 91.8%. [ABSTRACT FROM AUTHOR]

Here, FeAlOx catalytic deconstruction of polyethylene in a domestic microwave oven is reported. With the starting weight ratio of FeAlOx to polyethylene at 1:1, the concentration and yield of H2 reach up to 67.85 vol% and 48.1 mmol g−1plastic, respectively. CNTs@Fe3O4/Fe3C/Fe composite, which exhibits excellent microwave absorption properties, is generated simultaneously. The minimum reflection loss (RLmin) of the solid product reaches −54.78 dB at 15 GHz with an effective absorption bandwidth of 4.5 GHz at the thickness of 1.57 mm. [ABSTRACT FROM AUTHOR]

Available microwave notch-type damage detection sensors are typically based on monitoring frequency shift or magnitude changes. However, frequency shift testing needs sweep-frequency data that make scanning detection becomes difficult and time-consuming. This work presents a microwave near-field nondestructive testing sensor for detecting sub-millimeter notch-type damage detection in metallic surfaces. The sensor is loaded with an interdigital electrode element in an open-ended coaxial. It is simple to fabricate and inexpensive, as it is etched on the RC4003 patch by using printed circuit board technology. The detection is achieved by monitoring changes in reflection amplitude, which is caused by perturbing the electromagnetic field around the interdigital structure. The proposed sensor was tested on a metallic plate with different defects, and the experimental results indicated that the interdigital electrode probe can determine the orientation, localization and dimension of surface notch-type damage. [ABSTRACT FROM AUTHOR]

In this article, the effects of microwave frequency (2450 MHz and 5800 MHz) and gas humidity (1%, 2%, 3%, 4%, 6% and 8%) on in vitro blood coagulation with cold atmospheric pressure plasma (CAPP) were investigated. The generation of reactive oxygen species (ROS, OH, O) was measured by optical emission spectra. The exposure temperature on blood droplets under treatment was below 55 °C in all cases, to avoid the thermal effect of plasma on the blood clotting. Investigations showed that, with the increase of frequency, the doses of ROS increased, the blood sample presented a more serious collapse and its surface became drier. The humidity of ionized gas can also accelerate the generation of ROS and the process of blood clotting. Our results propose a method to accelerate in vitro blood coagulation in CAPP by adjusting microwave frequency and gas humidity, and suggest a clinical benefit for plasma treatment as a coagulation device in surgery. [ABSTRACT FROM AUTHOR]

As the problems of electromagnetic pollution and interference are becoming increasingly serious, the development of electromagnetic absorption materials with a high absorption capacity and broad absorption bandwidth are stringently needed. In this work, an N-doped 2D carbon/Ni complex is synthesized through direct microwave irradiation on a mixed solution of nickel nitrate, urea, and agarose under N2. The electromagnetic absorption performance can be tuned by controlling the Ni content. Specifically, minimum reflection loss values (RLmin) of −65.5 dB at 15.8 GHz with an effective absorption bandwidth (EAB) of 4.2 GHz at a sample thickness of 1.47 mm, and −55.4 dB at 11.8 GHz with an EAB of 3 GHz at a sample thickness of 1.92 mm can be obtained. The outstanding performance of electromagnetic absorption is attributed to the multiple polarization relaxation processes and the synergistic effect between 2D carbon sheets and Ni particles. [ABSTRACT FROM AUTHOR]

Microwave heating has been widely used in the chemical industry because of its advantages, such as fast heating rate, selective and controllable heating, increasing reaction rate and reducing by-products in chemical reactions. The Special Issue contains research on microwave applications in chemical engineering. [ABSTRACT FROM AUTHOR]

Conventional microwave heating has serious problems such as non-uniform heating and low efficiency. A novel magnetron microwave sweep frequency heating method is proposed to improve microwave heating uniformity. In this method, the frequency-sweeping signal is injected into the magnetron by the injection frequency-locking technique, and the microwave sweep frequency heating of the magnetron is realized. In this paper, a complicated injection frequency locking system is given and analyzed and a multiphysics calculation model based on the finite element method for electromagnetic waves and heat transfer is established. The calculation of microwave sweep frequency heating is realized by the combination of COMSOL and MATLAB. The results show that the sweep frequency heating has an obvious superiority. An experiment is carried out to verify the simulation results. The simulation results are in agreement with the experimental data. Moreover, the effect of sweep bandwidth and sweep interval on heating uniformity is discussed. [ABSTRACT FROM AUTHOR]

Microwave-assisted sintering materials have been proven to deliver improvements in the mechanical and physicochemical properties of the materials, compared with conventional sintering methods. Accurate values of dielectric properties of materials under high temperatures are essential for microwave-assisted sintering. In view of this, this paper, proposes an on-line system to measure the high temperature dielectric properties of materials under microwave processing at a frequency of 2450 MHz. A custom-designed ridge waveguide is utilized, where samples are heated and measured simultaneously. An artificial neural network (ANN) trained with the corresponding simulation data is integrated into this system to reverse the permittivity of the measured materials. This whole system is tested at room temperature with different materials. Accuracies of measuring dielectric property with an error lower than 9% with respect to theoretical data have been achieved even for high loss media. The functionality of the dielectric measurement system has also been demonstrated by heating and measuring Macor and Duran ceramic glass samples up to 800 °C. All the preliminary experiments prove the feasibility of this system. It provides another method for dielectric property measurement and improves the understanding of the mechanism between microwave and media under high temperatures, which is helpful for optimizing the microwave-assisted sintering of materials. [ABSTRACT FROM AUTHOR]

Oleic acid needs to be heated when it is utilized for biodiesel production, but, as a low-loss solution, oleic acid is difficult to heat by microwave. An efficient heating method for oleic acid is designed. A high loss material porous media is placed in a quartz tube, and a microwave directly heats the porous medium of the high loss material. The oleic acid flows through the pores of porous media so that the oleic acid exchanges heat during this process and rapid heating of oleic acid is achieved. A coupling model, based on the finite element method, is used to analyze the microwave heating process. The multiphysics model is based on a single mode cavity operating at 2450 MHz. An elaborate experimental system is developed to validate the multiphysics model through temperature measurements carried out for different flow velocities of oleic acid and different microwave power levels. The computational results are in good agreement with the experimental data. Based on the validated model, the effects of different sizes, porosities, and materials on microwave heating efficiency are analyzed. [ABSTRACT FROM AUTHOR]

Microwaves have been widely used in the treatment of different materials. However, the existing adjustable power thermostatic reactors cannot be used to analyze materials characteristics under microwave effects. In this paper, a microwave thermostatic chemical reactor for processing liquid materials is proposed, by controlling the velocity of coolant based on PLC (programmable logic controller) in different liquid under different constant electric field intensity. A nonpolar coolant (Polydimethylsiloxane), which is completely microwave transparent, is employed to cool the liquid materials. Experiments are performed to measure the liquid temperature using optical fibers, the results show that the precision of temperature control is at the range of ±0.5 °C. Compared with the adjustable power thermostatic control system, the effect of electric field changes on material properties are avoided and it also can be used to detect the properties of liquid materials and special microwave effects.

A number of studies have achieved the consensus that microwave thermal technology can regenerate the granular activated carbon (GAC) more efficiently and energy-conservatively than other technologies. In particular, in the microwave heating industry, permittivity is a crucial parameter. This paper developed two equivalent models to establish the relationship between effective complex permittivity and pore volume of the GAC. It is generally based on Maxwell-Garnett approximation (MGA) theory. With two different assumptions in the model, two quantificational expressions were derived, respectively. Permittivity measurements and Brunauer-Emmett-Teller (BET) testing had been introduced in the experiments. Results confirmed the two expressions, which were extremely similar. Theoretical and experimental graphs were matched. This paper set up a bridge which links effective complex permittivity and pore volume of the GAC. Furthermore, it provides a potential and convenient method for the rapid assisted characterization of the GAC in its adsorption performance.

Microwaves have been widely used in the treatment of materials, such as heating, drying, and sterilization. However, the heating in the commonly used microwave applicators is usually uneven. In this paper, a novel multi-material turntable structure is creatively proposed to improve the temperature uniformity in microwave ovens. Three customized turntables consisting of polyethylene (PE) and alumina, PE and aluminum, and alumina and aluminum are, respectively, utilized in a domestic microwave oven in simulation. During the heating process, the processed material is placed on a fixed Teflon bracket which covers the constantly rotating turntable. Experiments are conducted to measure the surface and point temperatures using an infrared thermal imaging camera and optical fibers. Simulated results are compared qualitatively with the measured ones, which verifies the simulated models. Compared with the turntables consisting of a single material, a 26%-47% increase in temperature uniformity from adapting the multi-material turntable can be observed for the microwave-processed materials.

Microwave processing of materials has been found to deliver enormous advantages over conventional processing methods in terms of mechanical and physical properties of the materials. However, the non-uniform temperature distribution is the key problem of microwave processing, which is related to the structure of the cavity, and the placement and physical parameters of the material. In this paper, a new microwave cavity structure with a sliding short based on phase-shifting heating is creatively proposed to improve the temperature uniformity. An electronic mathematical model based on the Finite Element Method (FEM) is built to predict the temperature distribution. Meanwhile, a new computational approach based on the theory of transformation optics is first provided to solve the problem of the moving boundary in the model simulation. At first, the experiment is carried out to validate the model, and heating results from the experiment show good agreement with the model's prediction. Based on the verified model, materials selected among a wide range of dielectric constants are treated by stationary heating and phase-shifting heating. The coefficient of variation (COV) of the temperature and temperature difference has been compared in detail between stationary heating and phase-shifting heating. A significant improvement in heating uniformity can be seen from the temperature distribution for most of the materials. Furthermore, three other materials are also treated at high temperature and the heating uniformity is also improved. Briefly, the strategy of phase-shifting heating plays a significant role in solve the problem of non-uniform heating in microwave-based material processing. A 25%-58% increase in uniformity from adapting the phase-shifting method can be observed for the microwave-processed materials.