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Fluid components in cores are crucial parameters in evaluating the quality of a shale reservoir in both laboratory analyses and log interpretation. In the Gulong area, shale reservoirs are characterized by a high clay content, with clay spaces hosting both oil and water phases, complicating the occurrence mechanism of fluid components, as a result, traditional research methods are no longer applicable. As an advanced technique, nuclear magnetic resonance (NMR) has been applied in oilfields to determine the specific petrophysical properties of rocks. To more accurately identify the types of fluid components, this study carried out a new, well-designed 2D NMR experiment, rock pyrolysis experiment, and quantitative oil and water detection experiment (QOWDE) to study the Gulong shale. This study measured the 2D NMR map of the original state, saturation state, centrifugal state, and pyrolysis at different temperatures, and conducted mutual verification between the QOWDE and 2D NMR pyrolysis experiments to obtain the distribution of different components of Gulong shale on the 2D NMR map. Based on the experimental results, this study developed a component identification template suitable for the Gulong area and calculated the 2D NMR porosity and saturation from it. This lays a foundation for the analysis and application of fluid components in the Gulong region and provides a new experimental basis and methodological support for porosity and saturation calculations. [ABSTRACT FROM AUTHOR]

Addressing the poor performance of existing logging saturation models in low-permeability tight sandstone reservoirs and the challenges in determining model parameters, this study investigates the pore structure and fluid occurrence state of such reservoirs through petrophysical experiments and digital rock visualization simulations. The aim is to uncover new insights into fluid occurrence state and electrical conduction properties and subsequently develop a low-permeability tight sandstone reservoir saturation model with easily determinable parameters. This model is suitable for practical oilfield exploration and development applications with high evaluation accuracy. The research findings reveal that such reservoirs comprise three types of formation water: strongly bound water, weakly bound water, and free water. These types are found in non-connected micropores, poorly connected mesopores where fluid flow occurs when the pressure differential exceeds the critical value, and well-connected macropores. Furthermore, the three types of formation water demonstrate variations in their electrical conduction contributions. By inversely solving rock electrical experiment data, it was determined that for a single sample, the overall cementation index is the highest, followed by the cementation index of pore throats containing strongly bound water, and the lowest for the pore throats with free water. Building on the aforementioned insights, this study develops a parallel electrical pore cementation index term, ϕm′, to account for the differences among the three types of water and introduces a parallel electrical saturation model suitable for logging evaluation of low-permeability tight oil and gas reservoirs. This model demonstrated positive application effects in the logging evaluation of low-permeability tight gas reservoirs in a specific basin in the Chinese offshore area, thereby confirming the advantages of its application. [ABSTRACT FROM AUTHOR]

Core samples of the tight sandstone reservoir in the Bonan Oilfield were analyzed by using multiple petrophysical experimental techniques, then a multi-scale three-dimensional digital rock model was constructed. The pore structure parameters of tight sandstone and homogeneous Berea sandstone were compared. The electrical simulation method based on the digital rock model was utilized to quantitatively reveal the influence of five micro-pore structure parameters (pore size, throat size, pore-throat size, coordination number, and shape factor) on the rock's electrical properties. In addition, the saturation of tight sandstone reservoirs was evaluated in combination with the three-component automatic mixed-connection conductivity model. The results show that the "non-Archie" phenomenon in sandstone is obvious, which is mainly caused by the small radius of the maximum connected pore throat and the complex structure of the pore throat. We noted that: with an increase in pore radius, throat radius, and coordination number, the formation factor decreases and tends to be stable; the pore-throat size increases and the formation factor decreases in the form of power function; the shape factor increases, and the formation factor increases; the larger the pore–throat ratio and shape factor, the greater the resistivity index; with an increase in coordination number, the resistivity index decreases; and the pore-throat size has no effect on the resistivity index. The calculation accuracy of oil saturation is improved by 6.54% by constructing the three-component automatic mixed-conductivity saturation model of tight sandstone. [ABSTRACT FROM AUTHOR]

The oil-based mud filtrate will invade the formation under the overbalanced pressure during drilling operations. As a result, alterations will occur to the nuclear magnetic resonance (NMR) response characteristics of the original formation, causing the relaxation time of the NMR T2 spectrum of the free fluid part to move towards a slower relaxation time. Consequently, the subsequent interpretation and petrophysical evaluation will be heavily impacted. Therefore, the actual measured T2 spectrum needs to be corrected for invasion. For this reason, considering the low-porosity and low-permeability of sandstone gas formations in the East China Sea as the research object, a new method to correct the incorrect shape of the NMR logging T2 spectrum was proposed in three main steps. First, the differences in the morphology of the NMR logging T2 spectrum between oil-based mud wells and water-based mud wells in adjacent wells were analyzed based on the NMR relaxation mechanism. Second, rocks were divided into four categories according to the pore structure, and the NMR logging T2 spectrum was extracted using the multidimensional matrix method to establish the T2 spectrum of water-based mud wells and oil-based mud wells. Finally, the correctness of the method was verified by two T2 spectrum correction examples of oil-based mud wells in the study area. The results show that the corrected NMR T2 spectrum eliminates the influence of oil-based mud filtrate and improves the accuracy of NMR logging for calculating permeability. [ABSTRACT FROM AUTHOR]

Some inter-salt shale reservoirs have high oil saturations but the soluble salts in their complex lithology pose considerable challenges to their production. Low-field nuclear magnetic resonance (NMR) has been widely used in evaluating physical properties, fluid characteristics, and fluid saturation of conventional oil and gas reservoirs as well as common shale reservoirs. However, the fluid distribution analysis and fluid saturation calculations in inter-salt shale based on NMR results have not been investigated because of existing technical difficulties. Herein, to explore the fluid distribution patterns and movable oil saturation of the inter-salt shale, a specific experimental scheme was designed which is based on the joint adaptation of multi-state saturation, multi-temperature heating, and NMR measurements. This novel approach was applied to the inter-salt shale core samples from the Qianjiang Sag of the Jianghan Basin in China. The experiments were conducted using two sets of inter-salt shale samples, namely cylindrical and powder samples. Additionally, by comparing the one-dimensional (1D) and two-dimensional (2D) NMR results of these samples in oil-saturated and octamethylcyclotetrasiloxane-saturated states, the distributions of free movable oil and water were obtained. Meanwhile, the distributions of the free residual oil, adsorbed oil, and kerogen in the samples were obtained by comparing the 2D NMR T1-T2 maps of the original samples with the sample heated to five different temperatures of 80, 200, 350, 450, and 600 °C. This research puts forward a 2D NMR identification graph for fluid components in the inter-salt shale reservoirs. Our experimental scheme effectively solves the problems of fluid composition distribution and movable oil saturation calculation in the study area, which is of notable importance for subsequent exploration and production practices. [ABSTRACT FROM AUTHOR]

It has been found that the relatively low abundance of gas hydrate in the Muli area of the Qilian Mountain causes gas hydrate reservoirs to have low-resistivity characteristics similar to those of low-resistivity oil and gas reservoirs. Therefore, it has great significance to research the main controlling factors affecting the electrical properties, and then come up a new logging identification and evaluation model for low-resistivity gas hydrate reservoirs. In this investigation, the rock samples of sandstone from gas hydrate reservoirs were scanned by CT and combined with gas hydrate distribution characteristics. The three-dimensional digital rocks with different hydrate saturation were constructed using the diffusion limited aggregation (DLA) model, and the resistivity was simulated via the finite element method. After sorting out the influencing factors of electrical characteristics, the sensitivity of the factors affecting electrical properties was evaluated using orthogonal analysis, using variance analysis and trend analysis to quantitatively evaluate the influencing factors of rock electrical sensitivity, so as to distinguish the main and secondary factors affecting rock electrical sensitivity. The results show that the sensitivity of rock electrical properties to the six influencing factors from strong to weak are: formation water salinity, water film thickness, shale content, conductive mineral content, micropores, and average coordination number. [ABSTRACT FROM AUTHOR]