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1. Measurement of thiamylal and thiopental in plasma by electron capture and flame photometric gas-liquid chromatography.

Author

Smith RH, MacDonald JA, Thompson DS, and Flacke WE

Subjects
Chromatography, Gas methods, Humans, Methods, Thiamylal blood, Thiopental blood
Abstract

We describe an isothermal gas-liquid chromatographic procedure developed for measuring thiamylal and thiopental in plasma. The unchanged drug is extracted into ethyl acetate from acidified plasma, together with an internal standard. The solvent is removed, the residue methylated, aliquots, diluted with benzene, are injected into a 183-cm gas-liquid chromatographic column containing 3% OV-17. Sensitivity of detection is in the nanogram to picogram range.

Published
1977

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