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The high-speed variability of the local water vapor content in the Earth atmosphere is a significant contributor to ground-based wavefront quality throughout the infrared domain. Unlike dry air, water vapor is highly chromatic, especially in the mid-infrared. This means that adaptive optics correction in the visible or near-infrared domain does not necessarily ensure a high wavefront quality at longer wavelengths. Here, we use literature measurements of water vapor seeing, and more recent infrared interferometric data from the Very Large Telescope Interferometer (VLTI), to evaluate the wavefront quality that will be delivered to the METIS mid-infrared camera and spectrograph for the Extremely Large Telescope (ELT), operating from 3 to 13 {\mu}m, after single-conjugate adaptive optics correction in the near-infrared. We discuss how the additional wavefront error due to water vapor seeing is expected to dominate the wavefront quality budget at N band (8-13 {\mu}m), and therefore to drive the performance of mid-infrared high-contrast imaging modes at ELT scale. Then we present how the METIS team is planning to mitigate the effect of water vapor seeing using focal-plane wavefront sensing techniques, and show with end-to-end simulations by how much the high-contrast imaging performance can be improved., Comment: 13 pages, paper presented at SPIE Astronomical Telescopes + Instrumentation 2022

Ground-based thermal-infrared observations have a unique scientific potential, but are also extremely challenging due to the need to accurately subtract the high thermal background. Since the established techniques of chopping and nodding need to be modified for observations with the future mid-infrared ELT imager and spectrograph (METIS), we investigate the sources of thermal background subtraction residuals. Our aim is to either remove or at least minimise the need for nodding in order to increase the observing efficiency for METIS. To this end we need to improve our knowledge about the origin of chop residuals and devise observing methods to remove them most efficiently, i.e. with the slowest possible nodding frequency. Thanks to dedicated observations with VLT/VISIR and GranTeCan/CanariCam, we have successfully traced the origin of three kinds of chopping residuals to (1) the entrance window, (2) the spiders and (3) other warm emitters in the pupil, in particular the VLT M3 mirror cell in its parking position. We conclude that, in order to keep chopping residuals stable over a long time (and therefore allow for slower nodding cycles), the pupil illumination needs to be kept constant, i.e. (imaging) observations should be performed in pupil-stabilised, rather than field-stabilised mode, with image de-rotation in the post-processing pipeline. This is now foreseen as the default observing concept for all METIS imaging modes., Comment: 17 pages, 9 figures, submitted to the SPIE proceedings as paper no. 11447-403

The Mid-Infrared ELT Imager and Spectrograph (METIS) is one of three first light instruments on the ELT. It will provide high-contrast imaging and medium resolution, slit-spectroscopy from 3 – 19um, as well as high resolution (R ~ 100,000) integral field spectroscopy from 2.9-5.3µm. All modes observe at the diffraction limit of the ELT, by means of adaptive optics, yielding angular resolutions of a few tens of milliarcseconds. The range of METIS science is broad, from Solar System objects to active galactic nuclei (AGN). We will present an update on the main science drivers for METIS: circum-stellar disks and exoplanets. The METIS project is now in full steam, approaching its preliminary design review (PDR) in 2018. In this paper we will present the current status of its optical, mechanical and thermal design as well as operational aspects. We will also discuss the challenges of building an instrument for the ELT, and the required technologies.

We present the preliminary design of the calibration unit of the future E-ELT instrument METIS. This independent subunit is mounted externally to the main cryostat of METIS and will function both as calibration reference for science observations, as well as verification and alignment tool during the AIT phase. In this paper, we focus on describing its preliminary layout and foreseen functionalities, based on the performance requirements defined at system level and the constraints imposed by warm IR background. We discuss the advantage of employing an integrating sphere as common radiation emitter, leading to a novel and versatile design, where the source's spatio-spectral properties can be varied with high fidelity and repeatability. By combining only few tuneable sources and mechanisms we show how a large instrument such as METIS can be calibrated and tested, without the need of a complex cold calibration unit.

METIS, a mid-infrared imager and spectrograph for the wavelength range 2.9–19μm (astronomical L-, M-, N- and Q-band), will be one of the first three science instruments at the European Extremely Large Telescope (E-ELT). It will provide diffraction limited imaging, coronagraphy, high resolution integral field spectroscopy and low and medium resolution slit spectroscopy. Within the international METIS consortium, the 1st Institute of Physics of the University of Cologne in Germany is responsible for the design, manufacturing, integration and qualification of the Warm Calibration Unit (WCU) of the instrument. The WCU will be a self-contained unit operating at ambient temperature outside of the voluminous METIS dewar, feeding a variety of optical calibration and alignment signals into the optical path of METIS. The functionalities of the WCU will be used for routine daily daytime calibrations after astronomical observing nights and verification of the internal alignment of METIS during assembly, integration and verification (AIV). In this contribution we present the preliminary optical design and principle of operation of the WCU in its current state of the preliminary design phase of METIS.

Sodium dodecyl sulfate polyacrylamide gel electrophoresis is a well-known technique to separate proteins by their molecular weight. After electrophoresis, the gels are commonly stained for protein band analysis with silver stain; this allows the detection of protein loads to about 1 ng. To increase the detection sensitivity of the protein bands down in the subnanogram level, a sensor has been developed based on the thermal lens effect to scan and quantify protein loads which would remain undetected using the standard imaging systems. The thermal lens sensor is equipped with a 450 nm diode pump laser modulated at 1 Hz and a HeNe probe laser mounted in collinear geometry. The sensor could detect protein bands of 0.05 ng when the gel was soaked in methanol/water and 0.1 ng in water. The limit of detection ranged from 8 to 20 pg, depending on the soaking medium and the staining efficiency. Thus, the detection of silver stain by thermal lens effect results 10 to 20 times more sensitive than the standard colorimetric method.

Organometallic halide perovskites CH3NH3BX3 (B= Pb, Sn, Ge; X = I, Br, Cl) have become one of the most promising semiconductors for solar cell applications, reaching power conversion efficiencies beyond 20%. Improving our ability to harness the full potential of organometal halide perovskites requires the development of more reliable synthesis routines of well defined, reproducible and defect free reference systems allowing to study the fundamental photo-physical processes. In this study we present size and band gap engineering for organo-lead perovskites crystallites with various shapes and sizes ranging from the 5 nm regime all the way to 1 cm. Colloidal nano-crystals, micro-crystlline particles as well as single crystals are demonstrated with excellent purity and control in shape and size are demonstrated. The structural, optical and photo-physical properties of these reference materials are investigated and analyzed as function of their size and shape.

Solution based perovskite solar cell fabrication typically involves rather complex processing sequences to yield highest performance. While most studies concentrate on the exploration of processing conditions, we have investigated the purity levels of common perovskite precursor solutions and found a number of impurities which are most critically controlling the crystallization of perovskites. Moreover, we identified these impurities at different level of concentrations is all commercially available precursors. In detail, we present a detailed chemical study on the nature of the various impurities in CH3NH3I and explored their impact on the crystal formation. The detrimental role of the impurities is best demonstrated by comparing perovskite solar cell devices fabricated from impurity free precursors vs precursors containing different concentrations of impurities. Most interestingly, we revealed that a certain concentration of impurities is detrimental to facilitate the growth of large grained crystals. This study gives valuable insight into the rate determining steps of perovskite crystal growth and provides the basis for developing reliable and reproducible high performance recipes for Perovskite solar cell processing.

METIS is one the first three instruments on the E-ELT. Apart from diffraction limited imaging, METIS will provide coronagraphy and medium resolution slit spectroscopy over the 3 – 19μm range, as well as high resolution (R ~ 100,000) integral field spectroscopy from 2.9 – 5.3μm, including a mode with extended instantaneous wavelength coverage. The unique combination of these observing capabilities, makes METIS the ideal instrument for the study of circumstellar disks and exoplanets, among many other science areas. In this paper we provide an update of the relevant science drivers, the METIS observing modes, the status of the simulator and the data analysis. We discuss the preliminary design of the optical system, which is driven by the need to calibrate observations at thermal IR wavelengths on a six-mirror ELT. We present the expected adaptive optics performance and the measures taken to enable high contrast imaging. We describe the opto-mechanical system, the location of METIS on the Nasmyth instrument platform, and conclude with an update on critical subsystem components, such as the immersed grating and the focal plane detectors. In summary, the work on METIS has taken off well and is on track for first light in 2025.

METIS is the Mid-infrared E-ELT Imager and Spectrograph, which will provide outstanding observing capabilities, focusing on high angular and spectral resolution. It consists of two diffraction-limited imagers operating in the LM and NQ bands respectively and an IFU fed diffraction-limited high-resolution (R=100,000) LM band spectrograph. These science subsystems are preceded by the common fore optics (CFO), which provides the following essential functionalities: calibration, chopping, image de-rotation, thermal background and stray light reduction. We show the evolution of the CFO optical design from the conceptual design to the preliminary optical design, detail the optimization steps and discuss the necessary trade-offs.

The Mid-infrared E-ELT Imager and Spectrograph (METIS) for the European Extremely Large Telescope (E-ELT) consists of diffraction-limited imagers that cover 3 to 14 microns with medium resolution (R ~ 5000) long slit spectroscopy, and an integral field spectrograph for high spectral resolution spectroscopy (R ~ 100,000) over the L and M bands. One of the science cases that METIS addresses is the characterization of faint circumstellar material and exoplanet companions through imaging and spectroscopy. We present our approach for high contrast imaging with METIS, covering diffraction suppression with coronagraphs, the removal of slowly changing optical aberrations with focal plane wavefront sensing, interferometric imaging with sparse aperture masks, and observing strategies for both the imagers and IFU image slicers.

We present the current status of the design of the science data reduction pipeline and the corresponding dataflow system for METIS. It will be one of the first three instruments for the E-ELT and work at wavelengths between 3-19 μm (L/M/N/Q1 bands). We will deliver software which is compliant to standards of the European Southern Observatory (ESO), and will employ state of the art techniques to produce science grade data, master calibration frames, quality control parameters and to handle instrument effects. The Instrument currently offers a wealth of observing modes that are listed in this paper. Data reduction for a ground based instrument at these wavelengths is particularly challenging because of the massive influence of thermal radiation from various sources. We will give a comprehensive overview of the data ow system for the imaging modes that the instrument offers and discuss a single recipe versus a multi recipe approach for the different observing modes for imaging.

METIS, the Mid-nfrared E-ELT Imager and Spectrometer, will be providing high-sensitivity imaging and high-resolution spectroscopy in the mid-infrared (3-19 micrometer) to the E-ELT. In order to achieve the exceptional performance required by its driving science cases, exoplanets and proto-planetary disks, METIS will be featuring two Adaptive Optics (AO) systems — a first-light Single Conjugate Adaptive Optics (SCAO) system, complemented by a Laser Tomographic Adaptive Optics (LTAO) system, most likely, a few years after first light. METIS, being one of the three first light science instruments on the European Extremely Large Telescope (E-ELT), will be one of the first instruments using the integrated deformable mirror of the E-ELT for its Adaptive Optics (AO) correction. The internal SCAO system designed to maximize the performance for bright targets and has its wavefront sensors (WFSs) build inside the METIS cryostat to minimize the number of warm surfaces towards the science detectors. Although the internal dichroic will reflect all light short wards of 3 micrometers towards the WFS, only the IR light will most likely be used, mainly due to the expected improved performance at longer wavelengths for the WFS. A trade-off has been made between both visible versus infrared wave front sensing as well as Pyramid versus Shack-Hartmann, under various observing conditions and target geometries, taking into account performance, target availability, reliability and technology readiness level. The base line for the SCAO system is to minimize system complexity, thereby ensuring system availability and reliability even under first-light conditions. Since the SCAO system will require a bright guide star near the science target, it can only be used for a limited number of targets. The LTAO system, consisting of up to 6 LGS and up to 3 low-order NGS WFS and located outside the cryostat, is designed to increase the sky coverage on arbitrary targets to >80%. Investigations are ongoing if the internal SCAO system can be used as either a Low-Order WFS or metrology system.

This paper discusses the development, realization and initial characterization of a demonstrator for a cryogenic 'set and forget' deformable mirror. Many optical and cryogenic infrared instruments on modern very and extremely large telescopes aim at diffraction-limited performance and require total wave front errors in the order of 50 nanometers or less. At the same time, their complex optical functionality requires either a large number of spherical mirrors or several complex free-form mirrors. Due to manufacturing and alignment tolerances, each mirror contributes static aberrations to the wave front. Many of these aberrations are not known in the design phase and can only be measured once the system has been assembled. A 'set-and-forget' deformable mirror can be used to compensate for these aberrations, making it especially interesting for systems with complex free-form mirrors or cryogenic systems where access to iterative realignment is very difficult or time consuming. The mirror with an optical diameter of 200 mm is designed to correct wave front aberrations of up to 2 μm root-mean square (rms). The shape of the wave front is approximated by the first 15 Zernike modes. Finite element analysis of the mirror shows a theoretically possible reduction of the wave front error from 2 μm to 53 nm rms. To produce the desired shapes, the mirror surface is controlled by 19 identical actuator modules at the back of the mirror. The actuator modules use commercially available Piezo-Knob actuators with a high technology readiness level (TRL). These provide nanometer resolution at cryogenic temperatures combined with high positional stability, and allow for the system to be powered off once the desired shape is obtained. The stiff design provides a high resonance frequency (>200 Hz) to suppress external disturbances. A full-size demonstrator of the deformable mirror containing 6 actuators and 13 dummy actuators is realized and characterized. Measurement results show that the actuators can provide sufficient stroke to correct the 2 μm rms WFE. The resolution of the actuator influence functions is found to be 0.24 nm rms or better depending on the position of the actuator within the grid. Superposition of the actuator influence functions shows that a 2 μm rms WFE can be accurately corrected with a 38 nm fitting error. Due to the manufacturing method of the demonstrator an artificially large print-through error of 182 nm is observed. The main cause of this print-through error has been identified and will be reduced in future design iterations. After these design changes the system is expected to have a total residual error of less than 70 nm and offer diffraction limited performance (λ14) for wavelengths of 1 μm and above.

Immersed gratings offer several advantages over conventional gratings: more compact spectrograph designs, and by using standard semiconductor industry techniques, higher diffraction-efficiency and lower stray-light can be achieved. We present the optical tests of the silicon immersed grating demonstrator for the Mid-infrared E-ELT Imager and Spectrograph, METIS. We detail the interferometric tests that were done to measure the wavefront-error and present the results of the throughput and stray-light measurements. We also elaborate on the challenges encountered and lessons learnt during the immersed grating demonstrator test campaign that helped us to improve the fabrication processes of the grating patterning on the wafer.