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We have expanded the pressure ranges at room and high temperatures generated in a Kawai-type multi-anvil apparatus (KMA) using tungsten carbide (WC) anvils with a high hardness ofHv = 2700 and a Young’s modulus of 660 GPa. At room temperature, a pressure of 64 GPa, which is the highest pressure generated with KMA using WC anvils in the world, was achieved using 1°-tapered anvils with a 1.5-mm truncation. Pressures of 48–50 GPa were generated at high temperatures of 1600–2000 K, which are also higher than previously achieved. Tapered anvils make wide anvil gaps enabling efficient X-ray diffraction. The present pressure generation technique can be used for studying the upper part of the Earth’s lower mantle down to 1200 km depth without sintered diamond anvils. [ABSTRACT FROM PUBLISHER]

We investigated phase relations in pyrolite at ∼33-40 GPa and ∼1800-2150 K by in situ X-ray diffraction using Kawai-type apparatus with sintered diamond anvils. The results demonstrated that MgSiO3-rich orthorhombic perovskite (mpv), CaSiO3-rich cubic perovskite (cpv) and (Mg,Fe)O ferropericlase (fp) are the stable phases in pyrolite bulk composition at the conditions corresponding to the lower mantle. However, chemical analyses of a run product recovered from ∼ 34 GPa by an analytical transmission electron microscope showed the coexistence of metallic iron particles with mpv, fp, and SiO2-rich amorphous phase. Also, Fe/Mg partitioning coefficient between mpv and fp was found to be 0.66(31), which is consistent with previous results for pyrolite bulk composition at 26-30 GPa and ∼1900 K. These results indicate that iron-rich metallic particles can exist in the lower mantle as a stable phase to the depth of at least ∼900 km. [ABSTRACT FROM AUTHOR]