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Objectives: Development of a new generation of stable β alloy, free of aluminum or vanadium and with better biological and mechanical compatibility and evaluate the surface properties of Ti-6Al-4V and Ti-35Nb-7Zr-5Ta after anodization in hydrofluoric acid, followed by deposition of different electrolyte concentrations of magnesium particles by micro arc-oxidation treatment., Methods: Disks were anodized in hydrofluoric acid. After this first anodization, the specimens received the deposition of magnesium using different concentration (8.5% and 12.5%) and times (30s and 60s). The surface morphology was assessed using scanning electron microscopy, and the chemical composition was assessed using energy dispersive x ray spectroscopy. The surface free energy was measured from the contact angle, and the mean roughness was measured using a digital profilometer., Results: Anodization in hydrofluoric acid provided the formation of nanotubes in both alloys, and the best concentration of magnesium considered was 8.5%, as it was the condition where the magnesium was incorporated without covering the morphology of the nanotubes. X-ray dispersive energy spectroscopy showed magnesium incorporation in all conditions. The average roughness was increased in the Ti-35Nb-7Zr-5Ta alloy., Conclusions: It was concluded that anodizing could be used to deposit magnesium on the surfaces of Ti-6Al-4V and Ti-35Nb-7Zr-5Ta nanotubes, with better results obtained in samples with magnesium concentration in 8.5% and the process favored the roughness in the Ti-35Nb-7Zr-5Ta group., (© 2020 The Author(s).)

Favorable results in the use of castor oil polyurethane (COP) as pulp capping, membrane material, sealer, mouthwash and in bone repair, associated with the fact that Ricinus communis is not derived from petroleum and it is abundant in Brazil, encourage researches in the development of luting agents. Objectives This study compared the flexural strength (FS) of a castor oil-containing dental luting agent with a weight percentage of 10% (wt%) of calcium carbonate (COP10) with RelyX ARC (RX) after mechanical cycling (MC) and distilled water storage. Material and Methods Sixty-four specimens (25x2x2 mm) were fabricated and divided into two groups, COP10 and RX (control). Each group was divided into 4 subgroups (n=8) according to the storage time, 24 hours (24 h) or 60 days (60 d), and the performance (MC+FS) or not (only FS) of the mechanical cycling test. The FS (10 kN; 0.5 mm/min) and MC tests (10,000 cycles, 5 Hz, 0.5 mm/min) were carried out using an MTS-810 machine. The data were analyzed using ANOVA (α=0.05). Results The obtained FS (MPa) values were: COP10 24h- 19.04±2.41; COP10 60d- 17.92±3.54; RX 24h- 75.19±3.43; RX 60d- 88.77±6.89. All the RX specimens submitted to MC fractured, while the values for COP10 after MC were as follows: COP10 24h- 17.90±1.87 and COP10 60d- 18.60±1.60. Conclusions A castor oil-containing dental luting agent with a weight percentage of 10% (wt%) of calcium carbonate is resistant to mechanical cycling without decreases in flexural strength. However, mean COP10 showed only about 25% of the RelyX ARC mean flexural strength.

Unlabelled: The need to develop new dental luting agents in order to improve the success of treatments has greatly motivated research., Objective: The aim of this study was to evaluate the diametral tensile strength (DTS) and film thickness (FT) of an experimental dental luting agent derived from castor oil (COP) with or without addition of different quantities of filler (calcium carbonate - CaCO3)., Material and Methods: Eighty specimens were manufactured (DTS N=40; FT N=40) and divided into 4 groups: Pure COP; COP 10%; COP 50% and zinc phosphate (control). The cements were mixed according to the manufacturers' recommendations and submitted to the tests. The DTS test was performed in the MTS 810 testing machine (10 KN, 0.5 mm/min). For FT test, the cements were sandwiched between two glass plates (2 cm²) and a load of 15 kg was applied vertically on the top of the specimen for 10 min. The data were analyzed by means of one-way ANOVA and Tukey's test (α=0.05)., Results: The values of DTS (MPa) were: Pure COP- 10.94 ± 1.30; COP 10%- 30.06 ± 0.64; COP 50%- 29.87 ± 0.27; zinc phosphate- 4.88 ± 0.96. The values of FT (µm) were: Pure COP- 31.09 ± 3.16; COP 10%- 17.05 ± 4.83; COP 50%- 13.03 ± 4.83; Zinc Phosphate- 20.00 ± 0.12. One-way ANOVA showed statistically significant differences among the groups (DTS - p=1.01E-40; FT - p=2.4E-10)., Conclusion: The experimental dental luting agent with 50% of filler showed the best diametral tensile strength and film thickness.

Objective: This study compared the cutting capacity of carbide burs sterilized with microwaves and traditional sterilization methods., Material and Methods: Sixty burs were divided into 5 groups according to the sterilization methods: dry heat (G1), autoclave (G2), microwave irradiation (G3), glutaraldehyde (G4) or control - no sterilization (G5). The burs were used to cut glass plates in a cutting machine set for twelve 2.5-min periods and, after each period, they were sterilized (except G5) following the protocol established for each group. The cutting capacity of the burs was determined by a weight-loss method. Data were analyzed statistically by Kruskal-Wallis and Dunn's test., Results: The means of the cutting amount performed by each group after the 12 periods were G1 = 0.2167 +/- 0.0627 g; G2 = 0.2077 +/- 0.0231 g; G3 = 0.1980 +/- 0.0326 g; G4 = 0.1203 +/- 0.0459 g; G5 = 0.2642 +/- 0.0359 g. There were statistically significant differences among the groups (p<0.05); only dry heat sterilization was similar to the control., Conclusion: Sterilization by dry heat was the method that least affected the cutting capacity of the carbide burs and microwave sterilization was not better than traditional sterilization methods.