10 results on '"Soenen, H."'
Search Results
2. Recommendation of RILEM TC 264 RAP on the evaluation of asphalt recycling agents for hot mix asphalt
- Author
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Hugener, M., Wang, D., Cannone Falchetto, A., Porot, L., Kara De Maeijer, P., Orešković, Marko, Sa-da-Costa, M., Tabatabaee, H., Bocci, E., Kawakami, A., Hofko, B., Grilli, A., Pasquini, E., Pasetto, M., Zhai, H., Soenen, H., Van den bergh, W., Cardone, F., Carter, A., Vasconcelos, K.L., Carbonneau, X., Lorserie, A., Mladenović, G., Koudelka, T., Coufalik, P., Zhang, R., Dave, E., Tebaldi, G., Hugener, M., Wang, D., Cannone Falchetto, A., Porot, L., Kara De Maeijer, P., Orešković, Marko, Sa-da-Costa, M., Tabatabaee, H., Bocci, E., Kawakami, A., Hofko, B., Grilli, A., Pasquini, E., Pasetto, M., Zhai, H., Soenen, H., Van den bergh, W., Cardone, F., Carter, A., Vasconcelos, K.L., Carbonneau, X., Lorserie, A., Mladenović, G., Koudelka, T., Coufalik, P., Zhang, R., Dave, E., and Tebaldi, G.
- Abstract
This recommendation is based on the results of an inter-laboratory study organised by the RILEM technical committee TC 264-RAP "Asphalt Pavement Recycling"—Task Group 3 (TG3) focusing on Asphalt Binder for Recycled Asphalt Mixture. The TG3 aimed to evaluate the effect of a specific family of materials known as asphalt recycling agent (ARA) on the aged binder under different configurations. Even though ageing is an irreversible phenomenon, effective ARA must have the capability to improve the flexibility of the bituminous materials and their resistance against cracking susceptibility with no adverse effect on the rutting resistance of pavements containing reclaimed asphalt. A total of 17 participating laboratories analysed the properties of binder blends composed of aged binder from reclaimed asphalt in three different contents (60, 80, 100%), ARA and virgin binder. The physical properties of the blends were thoroughly evaluated through traditional and rheological binder testing. This recommendation proposes to restore the original material properties at low and intermediate temperatures (i.e. cracking resistance) while balancing the high-temperature characteristics (i.e. rutting susceptibility) with durable impact throughout the progression of ageing phenomena. Therefore, useing of the Dynamic Shear Rheometer is foreseen as a more suitable and sustainable means to evaluate binder blends containing an asphalt recycling agent. Compared with conventional testing, the proposed approach requires fewer materials while resulting in a faster experimental procedure with one single test.
- Published
- 2022
3. Correction to: Recommendation of RILEM TC 264 RAP on the evaluation of asphalt recycling agents for hot mix asphalt (Materials and Structures, (2022), 55, 2, (31), 10.1617/s11527-021-01837-0)
- Author
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Hugener, M., Wang, D., Falchetto, A.C., Porot, L., De Maeijer, P.K., Orešković, Marko, Sa-da-Costa, M., Tabatabaee, H., Bocci, E., Kawakami, A., Hofko, B., Grilli, A., Pasquini, E., Pasetto, M., Zhai, H., Soenen, H., Van den bergh, W., Cardone, F., Carter, A., Vasconcelos, K.L., Carbonneau, X., Lorserie, A., Mladenović, G., Koudelka, T., Coufalik, P., Zhang, R., Dave, E., Tebaldi, G., Hugener, M., Wang, D., Falchetto, A.C., Porot, L., De Maeijer, P.K., Orešković, Marko, Sa-da-Costa, M., Tabatabaee, H., Bocci, E., Kawakami, A., Hofko, B., Grilli, A., Pasquini, E., Pasetto, M., Zhai, H., Soenen, H., Van den bergh, W., Cardone, F., Carter, A., Vasconcelos, K.L., Carbonneau, X., Lorserie, A., Mladenović, G., Koudelka, T., Coufalik, P., Zhang, R., Dave, E., and Tebaldi, G.
- Abstract
In this article the affiliation details for A. Kawakami were incorrectly given as ‘‘Department of Biological Information, Tokyo Institute of Technology, 4259 Nagatsuta, Midori-ku, Yokohama 226-8501, Japan’’ but should have been ‘‘Pavement Research Team, Public Works Research Institute, 1-6 Minamihara, Tsukuba-shi, Ibaraki-ken 305-8516, Japan’’. The original article has been corrected.
- Published
- 2022
4. Effect of Aging on the Rheological Properties of Blends of Virgin and Rejuvenated RA Binders
- Author
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Wang, D., Cannone Falchetto, A., Hugener, M., Porot, L., Kawakami, A., Hofko, B., Grilli, A., Pasquini, E., Pasetto, M., Tabatabaee, H., Zhai, H., da Costa, M.S., Soenen, H., Kara De Maeijer, P., Van den Bergh, W., Cardone, F., Carter, A., Vasconcelos, K.L., Carbonneau, X., Lorserie, A., Mladenović, G., Orešković, Marko, Koudelka, T., Coufalik, P., Bocci, E., Zhang, R., Dave, E.V., Tebaldi, G., Wang, D., Cannone Falchetto, A., Hugener, M., Porot, L., Kawakami, A., Hofko, B., Grilli, A., Pasquini, E., Pasetto, M., Tabatabaee, H., Zhai, H., da Costa, M.S., Soenen, H., Kara De Maeijer, P., Van den Bergh, W., Cardone, F., Carter, A., Vasconcelos, K.L., Carbonneau, X., Lorserie, A., Mladenović, G., Orešković, Marko, Koudelka, T., Coufalik, P., Bocci, E., Zhang, R., Dave, E.V., and Tebaldi, G.
- Abstract
The use of rejuvenators has seen a consistent increase over the years in the asphalt pavement industry. This is due to the need for maximizing the demand for incorporating a higher amount of Reclaimed Asphalt (RA) in the pavement asphalt mixtures. In order to tackle this challenge, the Task Group 3, focusing on asphalt binders and additives, of the RILEM TC RAP conducted an interlaboratory activity to evaluate the effect of aging on blends of virgin and rejuvenated RA binders. A set of conventional tests including penetration value at 25 °C, softening point temperature and rheological measurements by means of Dynamic Shear Rheometer (DSR) were selected to involve a large number of participants. A binder, recovered from field RA, was treated with a bio-based rejuvenator and blended with a virgin binder to simulate recycling at three different percentages 60, 80, and 100%. These blends, as well as the pure virgin binder, were next short and long term aged and tested to evaluate the changes in the corresponding properties. Relatively consistent results were obtained for the entire set of blends. The aging of combined rejuvenated RA and virgin binders was comparable to that experienced for the pure virgin binder. DSR data provided a more precise evolution of the impact of aging on the materials.
- Published
- 2022
5. Aging of Asphalt Symposium, September 17th 2014, Delft, the Netherlands
- Author
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Erkens, S.M.J.G., Scarpas, A., Blab, R., Glaser, R., Glover, C., Oeser, M., Porot, L., and Soenen, H.
- Subjects
asphalt ,aging ,tests ,procedures ,laboratory - Abstract
Technical specifications for the asphalt concrete properties are developed to be able to specify mixtures that will perform well in pavement applications. Being able to identify and determine properties related to pavement performance in practice is crucial for both road authorities and contractors, since it allows for design and risk management by determining design life times and reliability. However, the properties of Asphalt Concrete (AC) change over its lifetime and since most pavement layers last for a decade or more these changes are crucial in determining the performance in practice. For many of the standard materials the effect of aging is implicitly dealt with in the safety factors that also account for other effects such as the variation rest periods/healing and variations in traffic and weather in the design methods and specifications. Rapid changes in the materials used (increasing percentages reclaimed asphalt, bio-bitumen, rejuvenators, waste materials) and in the production of both bitumen (new refining methods resulting in different composition of bitumen) and asphalt concrete itself (warm mix asphalt, porous asphalt concrete, rubber asphalt mixtures) lead to increased uncertainty in the effects of aging. As a result, the uncertainties in pavement performance increase, which means the prediction of maintenance and the necessary budgets is getting more inaccurate. In order to maintain the ability to reliably design and maintain pavements and determine the most cost-effective solutions for a given situation, a better understanding of the aging processes and objective methods to take into account aging effects on material properties is needed. This need is widely recognized, in the USA the Mechanical Empirical Design Guide takes aging into account through aging tests on the bitumen used and in Europe CEN TC227 works on establishing a method to assess the aging sensitivity of asphalt mixtures. This symposium aimed at combining the existing information and insights from ongoing research into recommendations that will allow the development of methods to determine aging sensitivity and the impact on pavement performance, facilitate the exchange of obtained data and stimulate further developments The resulting recommendations are: Do make long term aging sensitivity of binders part of the bitumen standards and take the results from the aging sensitivity of binders into consideration when assessing AC properties. Be aware that RTFOT testing only gives an indication of the sensitivity of a penetration grade binder to aging during hot mix production and construction, it doesn’t work for hard grades, PMB’s or warm mixes. Because of the many variables involved, developing one test method to characterise aging sensitivity seems improbable. However, PAV aging is both practical and, if tests at various conditions are carried out, able to give kinematic properties. A PAV protocol for testing at two temperatures and time intervals could provide practical characterisation information for the short term and enable model development and validation on the long term. RCAT and other aging procedures could also be used in this sense, but considering the availability of equipment and the wide spread experience, PAV is the best candidate to allow the rapid development of international experience with the approach. Based on the current standards and the work presented during the symposium, PAV tests at 90 and 100 degrees Celsius and 20 and 40 hours, respectively, are suggested. The low values for temperature and duration are based on the current standards and fit both the USA and CEN procedure, while research shows that after 40 hours at 100 degrees the chemical (FTIR) and rheological (DSR) properties of laboratory aged and field samples were similar (Section 6.5 and 8.5). At 100oC the temperature is low enough so that the effect of secondary reactions is negligible. As such, these conditions are appropriate for kinetic expressions for in service pavement performance. For high temperature processes and possibly also for repeated recycling (very long term) more sophisticated methods are needed. Set-up and maintain field monitoring of temperature and UV radiation in various climate zones, as well as regular sampling over time and height to keep checking the predicted changes (from both tests and models), versus the actual changes in properties order to ensure reliability of the data as well as the applicability for pavement performance prediction. In setting up field tests, it is important to get both the composition of the virgin bitumen and the composition after mixing, transport and placement in the pavement. These compositions provide the starting points from both the material and pavement structure point of view and can be used to assess the development of aging products over time. There is a lot of discussion about the impact of binder recovery methods on the observed composition, so until it is proven that this does not have an influence, for comparisons the same recovery method should be used. Set up a coordination and support action on AC-Aging to continue to exchange information and experiences, both in research and in construction projects. develop an IR testing protocol, to facilitate the exchange of results and information. Compare the bitumen composition that is found through various recovery methods to establish if there is an effect and if so, develop a procedure to address this. To further understanding of aging, a Round Robin test on the differences in test conditions between US and EU, allowing better access to each other’s data and knowledge would be useful. When developing aging tests for AC, it would be useful to look at the US experience. As long as there is no fundamentally correct method for assessing the aging, it would be preferable to standardize it as much as possible in order to allow cooperation and exchange of data.
- Published
- 2015
6. Laboratory investigation of bitumen based on round robin DSC and AFM tests
- Author
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Soenen, H., Besamusca, J., Fischer, H.R., Poulikakos, L.D., Planche, J.P., Das, P.K., Kringos, N., Grenfell, J.R.A., Lu, X., and Chailleux, E.
- Subjects
Wax ,TS - Technical Sciences ,Industrial Innovation ,Bitumen ,Mechanics, Materials and Structures ,MIP - Materials for Integrated Products ,Asphalt ,Multiphase material ,AFM ,Materials ,DSC - Abstract
In the past years a wide discussion has been held among asphalt researchers regarding the existence and interpretation of observed microstructures on bitumen surfaces. To investigate this, the RILEM technical committee on nano bituminous materials 231-NBM has conducted a round robin study combining differential scanning calorimetry (DSC) and Atomic Force Microscopy (AFM). From this, methods for performing DSC and AFM tests on bitumen samples and determination of the influence of wax on the observed phases, taking into account thermal history, sample preparation and annealing procedure, are presented and critically discussed. DSC is used to measure various properties and phenomena that indicate physical changes such as glass transition temperature (T g) and phase transition such as melting and crystallization. In the case of existence of wax, either natural or synthetic, it can further indicate the melting point of wax, that could be used to determine wax content. The results from seven laboratories show that T g temperatures obtained from the heating scans are more repeatable and easier to obtain in comparison to the cooling scans. No significant difference was noted for T g's obtained from the first and second heating scans. AFM is an imaging tool used to characterize the microstructures on a bituminous surface. Using AFM three phases in the materials with wax could be distinguished. The changes in the phases observed with AFM for increases in temperature were correlated with the DSC curve, and it could be established that the so called "Bee" structure disappeared around the melting peak in the DSC curve. Thus, this research has confirmed the relation between the microstructures on a bitumen surface and the wax content. cop. 2013 RILEM.
- Published
- 2014
7. Aging of Asphalt Symposium, September 17th 2014, Delft, the Netherlands
- Author
-
Erkens, S.M.J.G. (author), Scarpas, A. (author), Blab, R. (author), Glaser, R. (author), Glover, C. (author), Oeser, M. (author), Porot, L. (author), Soenen, H. (author), Erkens, S.M.J.G. (author), Scarpas, A. (author), Blab, R. (author), Glaser, R. (author), Glover, C. (author), Oeser, M. (author), Porot, L. (author), and Soenen, H. (author)
- Abstract
Technical specifications for the asphalt concrete properties are developed to be able to specify mixtures that will perform well in pavement applications. Being able to identify and determine properties related to pavement performance in practice is crucial for both road authorities and contractors, since it allows for design and risk management by determining design life times and reliability. However, the properties of Asphalt Concrete (AC) change over its lifetime and since most pavement layers last for a decade or more these changes are crucial in determining the performance in practice. For many of the standard materials the effect of aging is implicitly dealt with in the safety factors that also account for other effects such as the variation rest periods/healing and variations in traffic and weather in the design methods and specifications. Rapid changes in the materials used (increasing percentages reclaimed asphalt, bio-bitumen, rejuvenators, waste materials) and in the production of both bitumen (new refining methods resulting in different composition of bitumen) and asphalt concrete itself (warm mix asphalt, porous asphalt concrete, rubber asphalt mixtures) lead to increased uncertainty in the effects of aging. As a result, the uncertainties in pavement performance increase, which means the prediction of maintenance and the necessary budgets is getting more inaccurate. In order to maintain the ability to reliably design and maintain pavements and determine the most cost-effective solutions for a given situation, a better understanding of the aging processes and objective methods to take into account aging effects on material properties is needed. This need is widely recognized, in the USA the Mechanical Empirical Design Guide takes aging into account through aging tests on the bitumen used and in Europe CEN TC227 works on establishing a method to assess the aging sensitivity of asphalt mixtures. This symposium aimed at combining the existing information a, Structural Engineering, Civil Engineering and Geosciences
- Published
- 2015
8. The influence of thermal history on binder rutting indicators
- Author
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UCL - FSA/AUCE - Département d'architecture, d'urbanisme et de génie civil environnemental, Soenen, H, Vanelstraete, Ann, Redelius, P, UCL - FSA/AUCE - Département d'architecture, d'urbanisme et de génie civil environnemental, Soenen, H, Vanelstraete, Ann, and Redelius, P
- Abstract
Binder properties, believed to relate to asphalt rutting, were investigated and compared with each other. Included are: parameters derived from oscillatory tests (e.g. the "zero" shear viscosity and the SHRP rutting parameter), parameters derived from static and repeated creep tests and the traditional R&B softening point. Various binders were tested, including low and high polymer modified bitumen, and bitumen modified with commercial waxes. This study shows that for unmodified bitumen all the investigated binder parameters correlate well with each other and would give similar classifications regarding the rutting susceptibility. For modified binders, the parameters related to low frequency or long loading times, give a different ranking than those related to higher frequencies, as for example the SHRP parameter. The storing and preparation conditions prior to the rheological measurement can have a large influence, especially in the range of long loading times or low frequencies. For elastomer modified binders, the homogenization temperature and the corresponding change in micro-structure can have a large impact. For binders with semicrystalline modifiers, the storage time and storage temperature before testing can introduce large changes in the polymer network building up. The thermal history effects in rheological tests can be related to variations in crystallinity, as shown by calorimetry, or to variations in morphology, as revealed by fluorescence microscopy. Some of the binders were also investigated in the presence of filler, to see if the thermal effects play a similar role in mastic (binder(+)filler) as in the neat binder.
- Published
- 2005
9. Dynamics and Structure of a Bitumen Emulsion as Studied by 1 H NMR Diffusometry.
- Author
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Filippov A, Soenen H, Blom J, and Antzutkin ON
- Abstract
Self-diffusion in a bitumen emulsion was studied by
1 H NMR. The emulsion forms two phases: continuous and dispersed. The continuous aqueous phase contains mainly water, with the energy of activation of the diffusion process equal to that of bulk water, while its diffusivity is smaller than that of bulk water by a factor of 2. The dispersed phase consists of bitumen droplets containing confined water, whose dynamics is characterized by a fully restricted diffusion regime in cavities with sizes of ∼0.11 μm. Therefore, the studied bitumen emulsion can be described by a model of a complex multiple emulsion of the water/oil/water (WOW) type. The suggested model does agree well with data from1 H NMR spectroscopy and diffusometry of the bitumen emulsion doped with paramagnetic MnSO4 (aq) as well as with an additional1 H NMR study of the emulsion structure, in which emulsion stability was compromised by freezing at 253 K., Competing Interests: The authors declare no competing financial interest., (© 2023 The Authors. Published by American Chemical Society.)- Published
- 2023
- Full Text
- View/download PDF
10. Neural crest cell survival is dependent on Rho kinase and is required for development of the mid face in mouse embryos.
- Author
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Phillips HM, Papoutsi T, Soenen H, Ybot-Gonzalez P, Henderson DJ, and Chaudhry B
- Subjects
- Actins genetics, Actins metabolism, Animals, Apoptosis physiology, Branchial Region abnormalities, Congenital Abnormalities genetics, Congenital Abnormalities metabolism, Craniofacial Abnormalities, Cytoskeleton genetics, Cytoskeleton metabolism, Face abnormalities, Mice, Mice, Transgenic, Neural Crest metabolism, rho-Associated Kinases genetics, Cell Survival physiology, Face embryology, Neural Crest cytology, rho-Associated Kinases metabolism
- Abstract
Neural crest cells (NCC) give rise to much of the tissue that forms the vertebrate head and face, including cartilage and bone, cranial ganglia and teeth. In this study we show that conditional expression of a dominant-negative (DN) form of Rho kinase (Rock) in mouse NCC results in severe hypoplasia of the frontonasal processes and first pharyngeal arch, ultimately resulting in reduction of the maxilla and nasal bones and severe craniofacial clefting affecting the nose, palate and lip. These defects resemble frontonasal dysplasia in humans. Disruption of the actin cytoskeleton, which leads to abnormalities in cell-matrix attachment, is seen in the RockDN;Wnt1-cre mutant embryos. This leads to elevated cell death, resulting in NCC deficiency and hypoplastic NCC-derived craniofacial structures. Rock is thus essential for survival of NCC that form the craniofacial region. We propose that reduced NCC numbers in the frontonasal processes and first pharyngeal arch, resulting from exacerbated cell death, may be the common mechanism underlying frontonasal dysplasia.
- Published
- 2012
- Full Text
- View/download PDF
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