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In this work, the microstructure evolution and magnetic properties of the 316LN austenitic stainless steels under high-cycle-fatigue loading at liquid helium temperature (4.2 K) were assessed by using the X-ray diffractometer (XRD), electron microscopy and magnetic measurements. The microstructure was composed of a single face-centered cubic (FCC) phase, and the high local misorientation was found near the grain boundaries. Observations through the high-resolution transmission electron microscopy reveals that the deformation was dominated by the dislocation and stacking faults. The magnetic susceptibility varies slightly after cyclic loading test at 4.2 K. [Display omitted] [ABSTRACT FROM AUTHOR]

• Mechanical properties of superconducting magnet insulation materials after reheat. • Strain responses during second Vacuum Pressure Impregnation process. • Monitoring by Fiber Bragg Grating sensors embedded in the insulation layers. • Additional strain introduced by the new added epoxy resin. In large-scale, high-field superconducting magnets used for magnetic confinement fusion, high energy accelerators, and magnetic resonance imaging, the insulating system made from glass fiber reinforced resin-based composites is the key component, which mainly plays the role of mechanical support, fixing and protecting superconducting conductors, as well as electrical insulation. Vacuum Pressure Impregnation (VPI) approach is widely used in the manufacturing of the insulation system. The second curing cycle is generally required after the first VPI and curing process. For example, after the superconducting coil is cured in the mold, the de-molding process requires the superconducting coil to be reheated according the curing temperature. Moreover, for large-scale superconducting magnets, the superconducting coil needs to undergo a second VPI process after the first VPI process to fix the coil in the coil case. In this work, the tensile and shear properties of pure epoxy resin and the glass fiber reinforced resin-based composite, were investigated at both room and cryogenic temperatures and the effect of the second curing cycle on the mechanical properties was analyzed. Additionally, the strain evolution of the Nb-Ti superconducting coil during the second curing cycle was measured using the Fiber Bragg Grating (FBG) sensors embedded in the composite. The results indicate that the second curing cycle will not introduce additional strain to the previously cured resin matrix, but the defective or weak parts of the resin matrix may be affected by the new added epoxy resin and a little extra strain has been observed. [ABSTRACT FROM AUTHOR]

• Mechanical properties of 316LN stainless steel with cryogenic pre-strain were studied at different temperatures (RT, 77 K and 4.2 K). • The pre-strained samples stretched at cryogenic temperature obtain higher mechanical strength. • The samples stretched at 77 K possess higher elongation and hardness than RT and 4.2 K, the mechanism was explained. • The results are attributed to the changes in dislocation density and martensite transformation due to temperature and cryogenic pre-strain. The 316LN stainless steel (SS) used for TF conduits in the ITER must undergo a series of pre-deformation during the fabrication. In order to investigate the variation of mechanical properties of 316LN SS with different temperature and cryogenic pre-strain, the cryogenic pre-strained samples with 0%, 15%, 25%, and 35% pre-strain were prepared and stretched at room temperature (RT), 77 K and 4.2 K, respectively. The yield strength (YS), ultimate tensile strength (UTS), elongation and microhardness of the samples were measured. Besides, the Scanning Electronic Microscopy (SEM) and Transmission Electronic Microscopy (TEM) were applied to observe the microstructure of 316LN SS. The magnetic measurements for the samples were carried out to investigate the volume percent of phase transformation. The results indicate that the YS, UTS and microhardness of 316LN SS are improved by means of cryogenic pre-strain and the decrease of elongation of pre-strained samples is different at different temperatures. All 316LN samples show the ductile fracture. The dislocation of samples promotes by cryogenic pre-strain and hinders by cryogenic temperatures. The martensitic transformation occurs after all pre-strained samples were stretched. The volume percent of α' martensite is minimal at RT and increases dramatically at cryogenic temperatures (77 K and 4.2 K). The combination of dislocation density and martensitic transformation results in changes in the 316LN SS mechanical properties. [ABSTRACT FROM AUTHOR]

Laser welding of modified 316LN steel with a thickness of 20 mm was conducted using a YLS-20000 fiber laser. The microstructure of the weld joint was characterized and tensile and fracture toughness tests were carried out. The microstructure evolution of the fracture specimens was studied systematically to elucidate the fracture mechanism. The weld was composed of the single austenite phase and was characterized by cellular and columnar grains, and the grain size became coarser with a weak orientation. The R m values of the laser welded joints were almost equal to that of the base metal both at RT and 4.2 K, and the fracture surfaces were featured by ductile fracture with quantities of dimples and microvoids. The fracture toughness of the weldments decreased to ˜84% of that of the parent metal at 4.2 K. Enhancement of the fracture toughness was attributed predominantly to the presence of twins and to the fine grain size, and the reduction was caused by the partially stress-induced phase transformation of the austenite to martensite. The synergistic effects of these factors result in a favorable improvement in the fracture toughness of the weldment. [ABSTRACT FROM AUTHOR]