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This investigation intends to come up with a cost-efficient and easily available bamboo leaf ash (BLA) which has high content of Silica, as an effective and complimenting reinforcement for the production of magnesium alloy-based metal matrix composites. By incorporating SiC and BLA reinforcement to AZ91D Mg alloy, the composites were made using the bottom pouring stir casting technique. The ratio between SiC and BLA in the composite, respectively, varied as 0:0, 6:0, 0:6, 4:2, 3:3, 2:4 wt.%. Fretting wear is one of the fundamental modes of wear for any mating parts which have vibration with low amplitude. In this study, an integrated Taguchi-TOPSIS is adapted to make the process variables more optimal for fretting wear of composites. Material composition, load, temperature, time, frequency and stroke length are selected as process parameters. The objective is to minimize the coefficient of friction, volume loss and surface roughness. Using the TOPSIS approach, the multi-criteria optimization approach was reduced to a single-criteria issue. The results revealed AZ91D/2 wt.% SiC/4 wt.% BLA, 10N, room temperature, 30-min, 30 Hz and 0.7 mm stroke as optimal parameters. Microscopic study demonstrates that fretting wear occurs in the partial slip zone for the composite tested at optimal condition. With temperature, the wear regime in composites shifts from partial slip to mixed fretting, whereas in alloys, the wear regime shifts from mixed fretting to gross slip. When the correct set of circumstances are available, hybrid composite can function well as a replacement for traditional materials in machineries vulnerable to fretting wear. [ABSTRACT FROM AUTHOR]

In the current study, graphite was exfoliated using a Hummer's technique to produce graphene oxide (GO), which was then reduced with hydrazine hydrate (a reducing agent) to produce reduced graphene oxide (rGO) with high purity. The XRD, FT-IR, SEM, and TGA analysis confirmed the synthesis of rGO by stating its crystal phase, chemical functional group, morphology, and thermal stability. The objective of this study is twofold: firstly, to synthesize the reduced graphene oxide (rGO) cost-effectively, and secondly, to explore its potential as an additional filler in Glass Fiber Reinforced Polymer (GFRP) composites. Aiming to enhance their overall performance. The GFRP laminate composite was fabricated through the hand layup technique by varying the concentration of Gr (i.e., 0.5 wt% & 1 wt%) and rGO (i.e., 0.5 wt% & 1 wt%). The morphological study of the fracture surface revealed a proper dispersion of filler obtained at 0.5 wt% and by increasing the concentration to 1 wt% it reveals a clustering of fillers and formation of micro-voids. The result revealed that maximum improvement has been observed in the GFRP composite having 0.5 wt% rGO composite than neat GFRP composite. Incorporation of rGO micro-filler in GFRP laminate composite significantly improved the tensile strength, flexural strength, and in their modulus by 59.56%, 18.21%, 24.45%, and 22.75% respectively compared to neat GFRP laminate composite. In the case of 0.5 wt% graphite filler demonstrates an enhancement in tensile strength, flexural strength, and their modulus by 37.98%, ∼8%, 6.64%, and ∼5% respectively. In fretting wear test reveals that 1 wt% of graphite filler has better wear resistance than all other composites. The worn morphology revealed adhesive and abrasive wear as the predominant wear mechanism. The incorporation of rGO filler in GFRP makes it a promising material for industrial applications that demand high strength and superior wear resistance. [ABSTRACT FROM AUTHOR]