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This article proposes an improved model-free deadbeat predictive current control (MFCC) method for permanent magnet synchronous motors (PMSMs) based on the ultralocal model and H∞ norm. Firstly, the traditional deadbeat predictive current control (DPCC) method is introduced and a theoretical analysis is conducted on its sensitivity to parameters. Building upon this, the limitations of model dependence and the limited robustness of the deadbeat predictive current control method based on the extended state observer (ESO-DPCC) are theoretically analyzed. Furthermore, an improved MFCC method based on the ultralocal model is proposed, and the influence of the observer on MFCC is theoretically analyzed. This study combined the proposed method with the H∞ norm, and the optimal coefficients of the observer were tuned to enhance the robustness and dynamic performance of the current loop. Finally, the proposed algorithms were validated on a 400 W PMSM platform. [ABSTRACT FROM AUTHOR]

To meet the environmental protection and flame retardancy requirements for epoxy resins (EPs) in certain fields, in this study, a novel triazine-ring-containing DOPO-derived compound (VDPD), derived from vanillin, 2,4-Diamino-6-phenyl-1,3,5-triazine, and 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO), was synthesized using a one-pot method. Flame-retardant epoxy resin (FREP) was prepared by adding various ratios of VDPD to EP and curing with 4,4-diaminodiphenylmethane (DDM). The curing behavior, thermal stability, mechanical properties, and flame-retardant properties of the FREP were examined in various tests. According to the results, when the amount of VDPD added to the EP increased, the glass transition temperature of the FREP decreased linearly, and the flame-retardant properties gradually improved. With a 0.4 wt.% P content, the vertical burning rating of EP/DDM/VDPD-0.4 (according to the theoretical content of VDPD) reached the V-0 level, and the LOI value reached 33.1%. In addition, the results of a CCT showed that the peak heat release rate (PHRR) of EP/DDM/VDPD-0.4 decreased by 32% in comparison with that of the EP. Furthermore, compared with those of the EP, the tensile strength of EP/DDM/VDPD-0.4 decreased from 80.2 MPa to 74.3 MPa, only decreasing by 6 MPa, and the tensile modulus increased. Overall, VDPD can maintain the mechanical properties of EP and effectively improve its flame-retardant properties. [ABSTRACT FROM AUTHOR]

Background: To establish a fast and simple quantitative method for detection of heart-type fatty acid-binding protein (H-FABP) in serum based on a background fluorescence quenching im munochromatographic assay. Methods: A detection card based on the double-antibody sandwich double-antibody method with background fluorescence quenching was developed for quantitative m easurement of H-FABP in serum. The optimal concentrations of control for coating the test and control lines were determined as well as the concentrations of gold-labeled antibodies used in preparing the detection system. The detection method for H-FABP in serum was established and validated using real-world clinical samples. Results: The optimal concentrations of labeling antibody and coating antibody were 5.0 mg/mL and 1.0 mg/m L, respectively. The test card had a sensitivity of 1.15 ng/m L over a linear concentration range of 0-100 ng/m L. Based on three batches prepared for testing the card, the relative standard deviation (RSD) within batches was less than 15% without a significant difference (P = 0.942 ). The detection method was tested against common interfering substances in serum, such as bilirubin, triglyceride and serum anticoagulants ethylenediamine tetraacetic acid (EDTA), heparin, and sodium citrate, and no significant cross-reaction was detected. The test method was further validated with 50 clinical serum samples, and the test results were COM parable with standard reference detection methods with good correlation (R = 0.95 ). Conclusion: O ur study presents a new method with strong specificity and sensitivity for the detection of H-FABP in serum, which could promote H-FABP detection in a broad range of applications.

Comprehensive Summary: Metal organic frameworks have been employed as high‐performance layered double hydroxide (LDH) composite supercapacitor electrode materials but have shown unsatisfactory redox ability and stability. Herein, a host‐guest CuMo‐based polyoxometalate‐based metal organic framework (POMOF) with copious electrochemically active sites and strong electrochemical redox activities has been effectively coupled with POM‐incorporated CoNi‐LDH to develop a nanocomposite (NENU‐5@CoNi‐LDH) by a simple solvothermal method. The designed electrode shows a high specific capacity of 333.61 mAh·g–1 at 1 A·g–1. In addition, the novel hybrid symmetric supercapacitor NENU‐5@CoNi‐LDH/active carbon (AC) demonstrated a high energy density of 80.8 Wh·kg–1 at a power density of 750.7 W·kg–1. Interestingly, the nanocomposite of NENU‐5@CoNi‐LDH exhibits an outstanding capacitance retention of 79% after 5000 charge‐discharge cycles at 10 A·g–1. This work provides a new strategy and will be the backbone for future energy storage research. [ABSTRACT FROM AUTHOR]

Comprehensive Summary: Metal organic frameworks have been employed as high‐performance layered double hydroxide (LDH) composite supercapacitor electrode materials but have shown unsatisfactory redox ability and stability. Herein, a host‐guest CuMo‐based polyoxometalate‐based metal organic framework (POMOF) with copious electrochemically active sites and strong electrochemical redox activities has been effectively coupled with POM‐incorporated CoNi‐LDH to develop a nanocomposite (NENU‐5@CoNi‐LDH) by a simple solvothermal method. The designed electrode shows a high specific capacity of 333.61 mAh·g–1 at 1 A·g–1. In addition, the novel hybrid symmetric supercapacitor NENU‐5@CoNi‐LDH/active carbon (AC) demonstrated a high energy density of 80.8 Wh·kg–1 at a power density of 750.7 W·kg–1. Interestingly, the nanocomposite of NENU‐5@CoNi‐LDH exhibits an outstanding capacitance retention of 79% after 5000 charge‐discharge cycles at 10 A·g–1. This work provides a new strategy and will be the backbone for future energy storage research. [ABSTRACT FROM AUTHOR]