1. Quantitative µ-CT Analysis of Scale Topology Formed During Oxidation of High SiMo Cast Iron
- Author
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Wesley Tucker, Asebi Bofah, Tara Selly, Semen Naumovich Lekakh, Tara Godlewski, and Mei Li
- Subjects
010302 applied physics ,Materials science ,Scale (ratio) ,020209 energy ,Metals and Alloys ,Oxide ,02 engineering and technology ,engineering.material ,Topology ,Combustion ,01 natural sciences ,Durability ,Inorganic Chemistry ,chemistry.chemical_compound ,Brittleness ,chemistry ,0103 physical sciences ,0202 electrical engineering, electronic engineering, information engineering ,Materials Chemistry ,engineering ,Cast iron ,Topology (chemistry) ,Water vapor - Abstract
High SiMo cast iron components in automotive exhaust systems are exposed to high-temperature oxidation over time. Quantitative analysis of formed oxide scale is therefore important for the assessment of a component durability. The brittle nature of multilayered scale and thermal stress limits capture of a true topology using traditional 2D destructive cut and polish methods. In this study, nondestructive high spatial-resolution 3D µCT analysis was performed on 2.90-mm-diameter oxidized specimens which permitted direct observation with 3.5 µm pixel resolution. The specimens were oxidized in three sequential time steps for a total 100 h at 700 °C and 800 °C in air and combustion gas atmospheres. A MATLAB-coded algorithm was used to quantify the topology, thickness variation in internal and external scale layers, and scale/metal interface unevenness. Scale topology was linked to oxidation temperature and gas atmosphere. A water vapor environment increases scale/metal interface unevenness and scale layer thickness irregularity which were related to an accelerated oxidation rate.
- Published
- 2020