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Objectives To investigate the wear resistance of polymers for injection molding, subtractive and additive manufacturing of occlusal devices in comparison with enamel antagonist wear and material properties (i.e., hardness, flexural strength, and flexural modulus). Methods Injection molding was compared with milling and the additive technologies stereolithography, low force stereolithography, and digital light processing. For each material, eight specimens were produced for wear measurements. Extracted human premolars served as indenters. All samples were subjected to two series of a 2-body wear test consisting of 200,000 circular loading cycles with an applied load of 1) 20 N and 2) 50 N in a thermocycling environment (5/55 °C, 30 s, 3860 cycles, H2O). Wear resistance was characterized by means of maximum depth and volume of the resulting traces. In addition, enamel wear of the indenters and Vickers hardness, flexural strength, and flexural modulus of the polymers were determined. Wear was statistically analyzed with linear general models for repeated measures and material properties with one-way ANOVA with post-hoc Tukey-HSD tests. Results Wear of the antagonists was not influenced by the material (P ≥ 0.343). Likewise, no differences in wear resistance were found between materials after cyclic loading with 20 N or 50 N (P ≥ 0.074). Material properties investigated revealed decreased values for the resins for the additive manufacturing with the exception of flexural strength of one material. Significance Within the limitations of this in-vitro study, arylates for conventional, subtractive, and additive manufacturing of occlusal devices differ in material properties but not in wear resistance and antagonist wear.

Additive manufacturing is becoming an increasingly important technique for the production of dental restorations and assistive devices. The most commonly used systems are based on vat polymerization, e.g., stereolithography (SLA) and digital light processing (DLP). In contrast, fused filament fabrication (FFF), also known under the brand name fused deposition modeling (FDM), is rarely applied in the dental field. This might be due to the reduced accuracy and resolution of FFF compared to vat polymerization. However, the use of FFF in the dental sector seems very promising for in-house production since it presents a cost-effective and straight forward method. The manufacturing of nearly ready-to-use parts with only minimal post-processing can be considered highly advantageous. Therefore, the objective was to implement FFF in a digital dental workflow. The present report demonstrates the production of surgical guides for implant insertion by FFF. Furthermore, a novel approach using a temperature-sensitive filament for bite registration plates holds great promise for a simplified workflow. In combination with a medical-grade filament, a multi-material impression tray was printed for optimized impression taking of edentulous patients. Compared to the conventional way, the printed thermoplastic material is pleasant to model and can allow clean and fast work on the patient.

To investigate the tensile and flexural strength of poured, subtractive, and additive manufactured denture base methacrylates bonded to soft and hard relining materials after hydrothermal cycling and microwave irradiation.This study included a conventional (CB), subtractive (SB), and additive (AB) base material as well as a soft (SCR) and hard (HCR) chairside and one hard laboratory-side (HLR) relining material. Reference bodies of the base materials and bonded specimens to the relining materials were produced with a rectangular cross-section. The specimens were either pre-treated by water storage (50 h, 37 °C), hydrothermal cycling (5000 cycles, 5 °C and 55 °C, 30 s each), or microwave irradiation (6 cycles, 640 W, 3 min, wet). A tensile and four-point bending test were performed for a total of 504 specimens. Data were analysed using multivariate analysis of variance (MANOVA) with post-hoc Tukey tests (α = 0.05).In comparison with the other reference groups SB showed marginally higher tensile and flexural strength (p0.047). Bond strength to SCR was affected neither by the base material nor by the pre-treatment (p0.085). HCR demonstrated twice the bond strength to AB compared with SB and CB (p ≤ 0.001). HLR showed the highest bond strength to CB (p ≤ 0.001). There was no difference between the specimens after hydrothermally cycling and microwave irradiation (p0.318).The bond strength of hard relining materials to subtractive and additive manufactured denture bases differ compared with conventional pouring.

Occlusal devices to reduce symptoms of bruxism and temperomandibular disorders can nowadays be manufactured in a digital workflow but studies comparing the accuracy of those occlusal devices are still limited. Therefore, the aim of this investigation was to investigate the accuracy of injection molding compared with four computer-aided design (CAD) and computer-aided manufacturing (CAM) techniques for the manufacturing of occlusal devices. In addition, the number of contact points and retention were evaluated to assess clinical relevance. A conventional workflow consisting of alginate impression, wax-up, and injection molding (IM) and digital workflows including intraoral scanning, digital design, and subtractive manufacturing (SM) or additive manufacturing by using stereolithography (SLA), digital light processing (DLP), and material jetting (Polyjet) were investigated. Sixteen splints were fabricated with each method. The intaglio surfaces of the splints were laser scanned and superimposed with the reference data sets to analyze the surface deviations. In addition, the number of contact points after repositioning the splints on the reference model was evaluated with occlusal foil. Finally, the retention was measured in a tensile test. One-way ANOVA with post hoc Tukey tests were used for statistical analyses (α = .05). IM and SM splints demonstrated the highest manufacturing accuracy without significant differences to each other (P .985). Additive manufactured splints revealed greater deviations with equal results for SLA and Polyjet (P .949) and significantly higher deviations for DLP compared to all other groups (P .002). Comparable retention force was measured for IM, SM, and SLA (P .923), whereas Polyjet splints showed the greatest variability. IM and SM splints presented the most contact points (P = .505). Additive manufactured splints demonstrated fewer contacts without significant difference to each other (P .116). It can be concluded, that there is no difference in manufacturing accuracy, retention, and number of contacts between IM and SM splints. AM splints demonstrated higher, however, clinically acceptable deviations.

OBJECTIVES: To evaluate two-body wear of three zirconia ceramics stabilized with 3, 4 and 5mol% yttria and to compare their wear behavior with that of a lithium-disilicate glass-ceramic. METHODS: Sixteen rectangular-shaped specimens made from three grades of zirconia ceramics and a lithium-disilicate glass-ceramic were polished and dynamically loaded in a chewing simulator (2kg vertical load, 2.1Hz) under water at 90°C for 1.2×106 cycles (about 7 days) in the ball-on-plate mode against steatite antagonists. Surface roughness was measured before and after wear testing. Wear tracks were scanned with a non-contact 3D profilometer and super-impositions were used to determine wear loss of the antagonists. Wear surfaces were imaged by SEM. XRD and micro-Raman spectroscopy were used to characterize phase transformation and stress status in the worn and unworn areas of the zirconia ceramics. RESULTS: Independent of fracture toughness, strength and aging-susceptibility, the three zirconia ceramics showed a similar and limited amount of wear (∼10μm in depth) and were more wear-resistant than the lithium-disilicate glass-ceramic (∼880μm in depth). Abrasive wear without obvious cracks was observed for all investigated zirconias, whereas the glass-ceramic with a lower fatigue threshold and high susceptibility to surface dissolution exhibited significant abrasion, fatigue and corrosion wear. All three zirconia ceramics yielded a lower antagonist wear than the glass-ceramic and no significant differences were found between the zirconia ceramics. SIGNIFICANCE: In the context of this study, high-translucent zirconia ceramics stabilized with a higher yttria content, recently introduced in the dental field, were as wear-resistant and antagonist-friendly as conventional high-strength zirconia and suitable for monolithic restorations. ispartof: DENTAL MATERIALS vol:35 issue:12 pages:1776-1790 ispartof: location:England status: published

Statement of problem Intraoral scanners (IOSs) are based on light-optical imaging methods. However, little is known about whether the ambient light in dental practices influences the accuracy and scanning time of the IOS. Purpose The purpose of this in vitro study was to investigate the influence of different illuminations on the accuracy of 4-unit and complete-arch scans of 6 IOSs. In addition, the required scanning time was evaluated. Material and methods A reference structure was attached to the first premolars (P) and second molars (M) in both quadrants (L/R) of a maxillary model. The resulting measured distances were M1-P1, M2-P2, P1-P2, and M1-M2. The investigation included 6 IOSs: TRIOS 3 (TRI), Cerec Omnicam (OC), iTero Element (ITE), CS 3600 (CS), Planmeca Emerald (EME), and GC Aadva (AAD). With each IOS, 17 scans at different illuminances (100, 500, 1000, and 5000 lux) were performed (N = 408). The precision and trueness for all distances were determined, and the scanning time was recorded. For statistical analyses, the Levene tests (precision) and 1-way analysis of variance with the post hoc Tukey honestly significant difference and Games-Howell tests (trueness) were calculated. Results Illuminance significantly influenced the trueness of 4-unit scans for OC, EME, and AAD. TRI, OC, ITE, and CS demonstrated comparable results. AAD (>96 ±22 μm; 1000 lux) and EME (>248 ±88 μm; 500 lux) revealed greater deviations. For complete-arch scans, illuminance did not influence TRI and AAD, but significant variations were detected for ITE, CS, EME, and AAD. The least deviations were achieved with TRI and OC. The scanning time was extended for all IOSs except ITE at more than 500 lux. The shortest scanning times with OC and EME were recorded at 100 lux; with TRI, CS, and AAD at 500 lux; and with ITE at both 100 and 5000 lux. At all illuminances, the fastest scans were obtained with TRI. Conclusions Ambient light was found to influence the accuracy and scanning time of IOSs. This influence varies depending on the device. For 4-unit scans, the effect was not clinically relevant, but for complete-arch scans, accuracy and scanning time can be improved with appropriate lighting.

OBJECTIVE: To investigate the fracture resistance and phase composition of tooth supported four-unit fixed dental prostheses (FDPs) made from three different zirconia grades after loading and aging. METHODS: Seventy-two FDPs were fabricated from 3Y-TZP, 4Y-PSZ and 5Y-PSZ. This resulted in 24 FDPs per grade, subdivided into three groups (n = 8): a control group (C), a hydrothermally aged (H2O, 85 °C, 90 days) group (A) and a group subjected to loading (2.5M cycles, 98N) with simultaneous thermal cycling (H2O, 5-55 °C) subsequent to treatment A (AL). Subsequently, FDPs were statically loaded to fracture. Phase composition was quantified by X-ray diffraction (XRD) and μ-Raman spectroscopy. Focused ion beam (FIB) - Scanning electron microscopy (SEM) was used for visualization in-depth. RESULTS: Compared to 3Y-C FDPs (1233 ± 165N), reduced fracture load was found for 5Y-C FDPs (889 ± 80 N; p < .001). This did not apply for 4Y-C samples (1065 ± 111N). Treatments (A, AL) did not negatively affect the fracture load for the three grades of zirconia (p > .645). Both A and AL increased monoclinic phase content for 3Y and 4Y FDPs, whereas FIB-SEM suggests no transformability of 5Y-PSZ. 5Y-AL FDPs showed cracks and fractures at the abutment walls and restoration margins after dynamic loading. Reduced fracture load of 5Y samples as compared to 3Y and 4Y was associated with deficient transformability in the fracture zone. SIGNIFICANCE: Aging and loading did not negatively affect the fracture resistance of monolithic four-unit FDPs made from three grades of zirconia. Due to cracks after dynamic loading, 5Y-PSZ cannot be recommended for the clinical application of four-unit FDPs. ispartof: DENTAL MATERIALS vol:36 issue:11 pages:E329-E339 ispartof: location:England status: published

Statement of problem Reliable studies comparing the accuracy of complete-arch casts from 3D printers are scarce. Purpose The purpose of this in vitro study was to investigate the accuracy of casts printed by using various extrusion- and photopolymerization-based printers. Material and methods A master file was sent to 5 printer manufacturers and distributors to print 37 identical casts. This file consisted of a standardized data set of a maxillary cast in standard tessellation language (STL) format comprising 5 reference points for the measurement of 3 distances that served as reference for all measurements: intermolar width (IMW), intercanine width (ICW), and dental arch length (AL). The digital measurement of the master file obtained by using a surveying software program (Convince Premium 2012) was used as the control. Two extrusion-based (M2 and Ultimaker 2+) and 3 photopolymerization-based printers (Form 2, Asiga MAX UV, and myrev140) were compared. The casts were measured by using a multisensory coordinate measuring machine (O-Inspect 422). The values were then compared with those of the master file. The Mann-Whitney U test and Levene tests were used to determine significant differences in the trueness and precision (accuracy) of the measured distances. Results The deviations from the master file at all 3 distances for the included printers ranged between 12 μm and 240 μm (trueness), with an interquartile range (IQR) between 17 μm and 388 μm (precision). Asiga MAX UV displayed the highest accuracy, considering all the distances, and Ultimaker 2+ demonstrated comparable accuracy for shorter distances (IMW and ICW). Although myrev140 operated with high precision, it displayed high deviations from the master file. Similarly, although Form 2 exhibited high IQR, it did not deviate significantly from the master file in the longest range (AL). M2 performed consistently. Conclusions Both extrusion-based and photopolymerization-based printers were accurate. In general, inexpensive printers were no less accurate than more expensive ones.

Concepts for digital denture manufacturing are market-available but studies comparing the trueness of such dentures, either milled (MIL) or additive manufactured, compared to injection molded (IM) ones are still limited. Regarding the impact of artificial aging and microwave sterilization on this parameter, no data are available. Therefore, the purpose of this investigation was to assess the trueness of IM, MIL, and stereolithography (SLA) printed denture bases after manufacturing, hydrothermal cycling, and microwave sterilization. Sixteen edentulous maxillary plaster models were poured using a silicone mold and digitized by means of a desktop scanner. For group IM, 16 denture bases were injection molded using these models. For group MIL and SLA, the denture bases were virtually designed and manufactured referring to the digitized data. A total of 48 samples were scanned 1) after manufacturing, 2) after hydrothermal cycling (5–55 °C, n = 5000), and after 3) three as well as 4) six cycles of microwave sterilization for 6 min each at 640 W. The 3-D surface deviation of the total intaglio surface, the palate, the alveolar ridge, and the border seal region was evaluated on the basis of the root mean square estimation (RMSE) and positive and negative mean deviations with an inspection software. For statistical analysis, ANOVA and post hoc Tukey tests were performed (α = 0.05). MIL showed the lowest deviations of the total RMSE (P ≤ .006) compared with the scans of the plaster models. In comparison, IM showed increased, mainly positive, deviations (P = .006) at the border seal. SLA presented the highest total RMSE (P = .001) with increased negative deviations, likewise at the border seal. In contrast to SLA (P = .001), no differences between IM and MIL (P = .816) were measured after hydrothermal cycling. Following microwave sterilization, the trueness of SLA was higher compared to IM and MIL (P = .001), with no differences between MIL and IM (P = .153). Distortion of IM and MIL was measured after the 3rd cycle with no further changes observed thereafter (P ≥ .385). It can be concluded, that subtractive manufacturing of denture bases results in the highest trueness, followed by IM and SLA. In contrast to IM and SLA, hydrothermal cycling did not affect MIL. Solely SLA printed denture bases remained dimensionally stable after microwave sterilization.