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1. Halocyclobutanol Dehydration En Route to Halocyclobutenes.

Author

Oeser, Petr, Petrenko, Artem, Edlová, Tereza, Čubiňák, Marek, Koudelka, Jakub, and Tobrman, Tomáš

Subjects
*DEHYDRATION, *ALLYL alcohol, *GRIGNARD reagents, *ALCOHOL drinking, *DICHLOROMETHANE, *ETHERS
Abstract

A new method for the preparation of halocyclobutenes is described. The developed process involves the dehydration of halocyclobutanols by using tetrafluoroboric acid–diethyl ether complex in dichloromethane at room temperature. The process allows for high yields of halocyclobutenes to be achieved by using alcohols that do not trigger the formation of isomeric allylic halides. [ABSTRACT FROM AUTHOR]

Published
2022
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